1CIC
IDIOTOPE-ANTI-IDIOTOPE FAB-FAB COMPLEX; D1.3-E225
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 293 |
| Detector technology | AREA DETECTOR |
| Collection date | 1987-11 |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 75.110, 77.650, 96.750 |
| Unit cell angles | 90.00, 111.80, 90.00 |
Refinement procedure
| Resolution | 7.000 - 2.500 |
| R-factor | 0.179 * |
| Rwork | 0.179 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | FAB D1.3 |
| RMSD bond length | 0.016 |
| RMSD bond angle | 0.042 |
| Data reduction software | ROTAVATA |
| Data scaling software | CCP4 ((AGROVATA) |
| Phasing software | AMoRE |
| Refinement software | PROFFT |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 13.700 |
| High resolution limit [Å] | 2.500 |
| Rmerge | 0.076 |
| Number of reflections | 33526 |
| Completeness [%] | 97.0 |
| Redundancy | 2.84 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.9 | 12% PEG 800, 75 MILLIMOLAR SODIUM ACETATE PH 4.85 10MGM/ML PROTEIN CONCENTRATION , pH 4.9 |
