1C9Z
D232-CGTACG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 300 |
Detector technology | AREA DETECTOR |
Collection date | 1995-09-09 |
Detector | UCSD MARK II |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 28.240, 28.240, 72.744 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.400 |
R-factor | 0.1961 |
Rwork | 0.196 |
R-free | 0.19610 |
RMSD bond length | 0.021 * |
RMSD bond angle | 3.290 * |
Data reduction software | SDMS |
Data scaling software | SDMS |
Phasing software | MADSYS |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 | 2.510 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.051 | 0.060 |
Total number of observations | 5220 * | |
Number of reflections | 744 * | |
<I/σ(I)> | 9.2 | |
Completeness [%] | 91.0 | 84 |
Redundancy | 3.2 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 300 | MPD, SPERMINE, MAGNESIUM CHLORIDE, SODIUM CACODYLATE, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 300K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | SPERMINE | ||
2 | 1 | 1 | MGCL2 | ||
3 | 1 | 1 | SODIUM CACODYLATE | ||
4 | 1 | 1 | MPD | ||
5 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA single strand | 0.8 (mM) | |
2 | 1 | drop | sodium cacodylate | 15.8 (mM) | |
3 | 1 | drop | MPD | 2.6 (%) | |
4 | 1 | drop | spermine | 0.51 (mM) | |
5 | 1 | drop | 0.66 (mM) | ||
6 | 1 | drop | D232 | 0.37 (mM) | |
7 | 1 | reservoir | MPD | 20 (%) |