1BZ1
HEMOGLOBIN (ALPHA + MET) VARIANT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 295 |
Detector technology | AREA DETECTOR |
Collection date | 1992-09-18 |
Detector | SDMS |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.300, 83.600, 53.800 |
Unit cell angles | 90.00, 99.40, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.590 |
R-factor | 0.17 * |
Rwork | 0.170 |
R-free | 0.22400 |
Structure solution method | OTHER |
Starting model (for MR) | HBA STRUCTURE PDB FILE IN BNL-25483 |
RMSD bond length | 0.013 |
RMSD bond angle | 0.030 |
Data reduction software | SDMS |
Data scaling software | SDMS |
Phasing software | X-PLOR |
Refinement software | PROLSQ |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 1.720 |
High resolution limit [Å] | 1.590 | 1.590 |
Rmerge | 0.053 | 0.196 |
Total number of observations | 399325 * | |
Number of reflections | 61802 | |
<I/σ(I)> | 14 | 2.48 |
Completeness [%] | 83.9 | 66.6 |
Redundancy | 6.5 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * | 6.5 | 2.3 M AMMONIUM SULFATE 0.3 M AMMONIUM PHOSPHATE PH 6.5 10 MM FERROUS CITRATE |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ammonium phosphate | 10 (mM) |