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1BVI

RIBONUCLEASE T1 (WILDTYPE) COMPLEXED WITH 2'GMP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]293
Detector technologyIMAGE PLATE
Collection date1997-12-15
DetectorMARRESEARCH
Spacegroup nameP 21 21 21
Unit cell lengths59.340, 60.590, 100.930
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution20.000 - 1.900
R-factor0.177
Rwork0.177
R-free0.21900
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1rga
RMSD bond length0.006
RMSD bond angle24.650

*

Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareX-PLOR
Refinement softwareX-PLOR (3.851)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0001.990
High resolution limit [Å]1.9001.900
Rmerge0.061

*

Total number of observations138761

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Number of reflections28421
<I/σ(I)>15.864.75
Completeness [%]96.777.1
Redundancy4.883.26
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1unknown

*

4.225 MM NAAC PH 4.2 6.25 MM CACL2 47.5 % MPD
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
111protein10 (mg/ml)
21125 (mM)
3112'GMP2.8 (mM)
4116.25 (mM)
511MPD47.5 (%)

229380

PDB entries from 2024-12-25

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