1BND

STRUCTURE OF THE BRAIN-DERIVED NEUROTROPHIC FACTOR(SLASH)NEUROTROPHIN 3 HETERODIMER

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1994-01-04
Detector	MARRESEARCH
Spacegroup name	C 1 2 1
Unit cell lengths	98.400, 45.100, 68.000
Unit cell angles	90.00, 118.30, 90.00

Refinement procedure

Resolution	20.000 - 2.300
R-factor	0.182
Rwork	0.182
RMSD bond length	0.015
RMSD bond angle	1.890
Data reduction software	DENZO
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000 *
High resolution limit [Å]	2.300 *	2.300 *
Rmerge	0.082	0.150 *
Number of reflections	11691 *	1455 *
Completeness [%]	93.4	85.6 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *	5.6 *	18 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	15 (mg/ml)
2	1	reservoir	PEG4000	10 (%(w/v))
3	1	reservoir	2-propanol	10 (%(v/v))
4	1	reservoir	sodium citrate	0.1 (M)