1BCS

COMPLEX OF THE WHEAT SERINE CARBOXYPEPTIDASE, CPDW-II, WITH THE MICROBIAL PEPTIDE ALDEHYDE INHIBITOR, CHYMOSTATIN, AND ARGININE AT 100 DEGREES KELVIN

Experimental procedure

Temperature [K]	100
Detector technology	IMAGE PLATE
Detector	RIGAKU
Spacegroup name	P 41 21 2
Unit cell lengths	95.400, 95.400, 208.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.000 - 2.100 *
R-factor	0.174
RMSD bond length	0.016
RMSD bond angle	2.800 *
Data reduction software	R-AXIS
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.100 *	2.100 *
Rmerge	0.040
Total number of observations	127152 *
Number of reflections	46630 *
Completeness [%]	81.0 *	23 *
Redundancy	2.75

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop		100 (mM)
2	1	drop	PEG4000	0.2 (%(w/v))
3	1	reservoir	sodium chloride	1.25 (M)
4	1	reservoir	sodium acetate	50 (mM)
5	1	drop	sodium acetate	50 (mM)