1B71

RUBRERYTHRIN

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Temperature [K]	298
Detector technology	AREA DETECTOR
Detector	XUONG-HAMLIN MULTIWIRE
Spacegroup name	I 2 2 2
Unit cell lengths	49.300, 81.300, 100.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 1.900
R-factor	0.195
Structure solution method	OTHER
Starting model (for MR)	PDB IDENTIFIER 1RYT
RMSD bond length	0.006
Refinement software	SHELXL-97

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	1.900
Rmerge	0.093
Number of reflections	15420
<I/σ(I)>	9.4
Completeness [%]	94.8
Redundancy	15.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	8		pH 8

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	TRIZMA hydrochloride	0.1 (M)
2	1	reservoir	PEG1450	15 (%)