1AND
ANIONIC TRYPSIN MUTANT WITH ARG 96 REPLACED BY HIS
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 273 |
Detector technology | AREA DETECTOR |
Collection date | 1992 |
Detector | SIEMENS |
Spacegroup name | I 2 3 |
Unit cell lengths | 124.380, 124.380, 124.380 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.300 |
R-factor | 0.161 |
Rwork | 0.161 |
RMSD bond length | 0.013 |
RMSD bond angle | 2.900 |
Data reduction software | BUDDHA |
Data scaling software | BUDDHA |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 |
Rmerge | 0.070 * |
Total number of observations | 26500 * |
Number of reflections | 13200 |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 | pH 8.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | 22 (%(w/v)) | ||
2 | 1 | reservoir | Tris-HCl | 20 (mM) |