1AK2
ADENYLATE KINASE ISOENZYME-2
Experimental procedure
| Source type | ROTATING ANODE |
| Detector technology | AREA DETECTOR |
| Collection date | 1992 |
| Detector | SIEMENS-NICOLET X100 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 44.200, 50.100, 122.300 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.920 |
| R-factor | 0.222 |
| Rwork | 0.222 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.600 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 10.000 |
| High resolution limit [Å] | 1.920 |
| Rmerge | 0.077 |
| Number of reflections | 20850 |
| Completeness [%] | 98.0 |
| Redundancy | 13 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | PEG | precipitant |
