1AI1

HIV-1 V3 LOOP MIMIC

Experimental procedure

Temperature [K]	287
Detector technology	IMAGE PLATE
Collection date	1995-08
Detector	MARRESEARCH
Spacegroup name	C 2 2 21
Unit cell lengths	89.930, 154.430, 121.460
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	12.000 - 2.800
R-factor	0.22
Rwork	0.220
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1acy
RMSD bond length	0.015 *
RMSD bond angle	2.000 *
Data reduction software	MOSFLM
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]		2.900
High resolution limit [Å]	2.800	2.800
Rmerge	0.080 *
Total number of observations	50028 *
Number of reflections	19192
Completeness [%]	92.0	90

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *	6.5	22 *	pH 6.5

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	sodium potassium phosphate	1.4-1.8 (M)
2	1	drop	Fab	15 (mg/ml)