1AD4

DIHYDROPTEROATE SYNTHETASE COMPLEXED WITH OH-CH2-PTERIN-PYROPHOSPHATE FROM STAPHYLOCOCCUS AUREUS

Experimental procedure

Temperature [K]	120
Collection date	1996-08
Spacegroup name	P 1 21 1
Unit cell lengths	65.748, 42.142, 99.040
Unit cell angles	90.00, 106.06, 90.00

Refinement procedure

Resolution	13.000 - 2.400
R-factor	0.176
Rwork	0.176
RMSD bond length	0.012
RMSD bond angle	1.800
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	13.000 *
High resolution limit [Å]	2.400 *	2.400 *
Rmerge	0.060 *
Total number of observations	57389 *
Number of reflections	19669 *
Completeness [%]	93.0 *	88 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *		4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG4000	12-16 (%(v/w))
2	1	reservoir	sodium potassium tartrate	200 (mM)
3	1	reservoir	bis-tris	100 (mM)