1A9C
GTP CYCLOHYDROLASE I (C110S MUTANT) IN COMPLEX WITH GTP
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 280 |
| Detector technology | IMAGE PLATE |
| Collection date | 1996-01-06 |
| Detector | MARRESEARCH |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 313.900, 226.800, 131.400 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.900 |
| R-factor | 0.206 |
| Rwork | 0.206 |
| R-free | 0.28800 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.720 |
| Data reduction software | MOSFLM |
| Phasing software | X-PLOR (3.8) |
| Refinement software | X-PLOR (3.8) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 25.000 |
| High resolution limit [Å] | 2.900 |
| Rmerge | 0.082 |
| Number of reflections | 86307 |
| Completeness [%] | 84.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | pH 7.0 |
