192D
RECOMBINATION-LIKE STRUCTURE OF D(CCGCGG)
Experimental procedure
Source type | ROTATING ANODE |
Source details | ELLIOTT GX-21 |
Detector technology | DIFFRACTOMETER |
Detector | OTHER |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 34.330, 44.040, 38.270 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.920 |
R-factor | 0.185 |
Rwork | 0.185 |
RMSD bond length | 0.016 |
RMSD bond angle | 3.280 |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.920 |
Rmerge | 0.056 * |
Total number of observations | 13022 * |
Number of reflections | 2297 |
Completeness [%] | 96.5 * |
Redundancy | 5.7 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | pH 6.00, VAPOR DIFFUSION, SITTING DROP |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | SPERMINE | ||
4 | 1 | 1 | TETRA-ARGININE | ||
5 | 1 | 1 | NA CACODYLATE | ||
6 | 1 | 2 | WATER | ||
7 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | hexanucleotide | 0.83 (mM) | |
2 | 1 | drop | spermine | 2.8 (mM) | |
3 | 1 | drop | tetra arginine | 0.6 (mM) | |
4 | 1 | drop | sodium ccacodylate | 18 (mM) | |
5 | 1 | drop | MPD | 20 (%(v/v)) | |
6 | 1 | reservoir | MPD | 45 (%) |