183D
X-RAY STRUCTURE OF A DNA DECAMER CONTAINING 7, 8-DIHYDRO-8-OXOGUANINE
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 277 |
Detector technology | AREA DETECTOR |
Detector | SDMS |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 32.270, 25.560, 34.710 |
Unit cell angles | 90.00, 115.77, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.600 |
R-factor | 0.234 |
Rwork | 0.234 |
RMSD bond length | 0.020 |
RMSD bond angle | 3.600 |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.600 |
Rmerge | 0.055 * |
Number of reflections | 3290 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.6 | 4 * | pH 7.60, VAPOR DIFFUSION, SITTING DROP, temperature 277.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | BIS-TRIS-PROPANE_HCL | ||
4 | 1 | 1 | MGCL2 | ||
5 | 1 | 2 | WATER | ||
6 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA | 1.9 (mM) | single stranded |
2 | 1 | drop | Tris-HCl | 20 (mM) | |
3 | 1 | drop | methylpentanediol | 5 (%) | |
4 | 1 | drop | 133 (mM) | ||
5 | 1 | reservoir | methylpentanediol | 30 (%) |