17GS

GLUTATHIONE S-TRANSFERASE P1-1

Experimental procedure

Source type	ROTATING ANODE
Source details	RIGAKU RUH2R
Temperature [K]	288
Detector technology	IMAGE PLATE
Collection date	1996-03-20
Detector	MARRESEARCH
Spacegroup name	C 1 2 1
Unit cell lengths	79.213, 90.228, 69.254
Unit cell angles	90.00, 98.61, 90.00

Refinement procedure

Resolution	15.000 - 1.900
R-factor	0.174
Rwork	0.174
R-free	0.20000
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5gss
RMSD bond length	0.006
RMSD bond angle	1.300
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	X-PLOR (3.851)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	1.930
High resolution limit [Å]	1.900	1.900
Rmerge	0.080	0.187
Number of reflections	31937
<I/σ(I)>	11.4	3.78
Completeness [%]	84.1	59
Redundancy	2.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6.6		pH 6.6