15C8
CATALYTIC ANTIBODY 5C8, FREE FAB
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | MACSCIENCE M06X |
| Temperature [K] | 293 |
| Detector technology | AREA DETECTOR |
| Collection date | 1996-11 |
| Detector | SIEMENS |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 201.000, 80.500, 39.300 |
| Unit cell angles | 90.00, 98.70, 90.00 |
Refinement procedure
| Resolution | 30.000 - 2.500 |
| R-factor | 0.19 |
| Rwork | 0.190 |
| R-free | 0.25100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1dbb |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.300 |
| Data reduction software | XENGEN |
| Data scaling software | XENGEN |
| Phasing software | AMoRE |
| Refinement software | X-PLOR (3.851) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.590 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 20624 | |
| <I/σ(I)> | 17.7 | 1.6 |
| Completeness [%] | 95.6 | 84.1 |
| Redundancy | 2.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.5 | pH 5.5 |
