158D
CRYSTALLOGRAPHIC ANALYSIS OF C-C-A-A-G-C-T-T-G-G AND ITS IMPLICATIONS FOR BENDING IN B-DNA
Experimental procedure
Temperature [K] | 278 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 6 |
Unit cell lengths | 53.080, 53.080, 34.320 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 1.900 |
R-factor | 0.179 |
RMSD bond length | 0.016 * |
RMSD bond angle | 0.034 * |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.900 |
Number of reflections | 4095 |
Completeness [%] | 89.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 278 | pH 7.50, VAPOR DIFFUSION, temperature 278.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | CA ACETATE | ||
4 | 1 | 2 | WATER | ||
5 | 1 | 2 | MPD |