158D
CRYSTALLOGRAPHIC ANALYSIS OF C-C-A-A-G-C-T-T-G-G AND ITS IMPLICATIONS FOR BENDING IN B-DNA
Experimental procedure
| Temperature [K] | 278 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS II |
| Spacegroup name | P 6 |
| Unit cell lengths | 53.080, 53.080, 34.320 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 1.900 |
| R-factor | 0.179 |
| RMSD bond length | 0.016 * |
| RMSD bond angle | 0.034 * |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 1.900 |
| Number of reflections | 4095 |
| Completeness [%] | 89.0 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.5 | 278 | pH 7.50, VAPOR DIFFUSION, temperature 278.00K |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | MPD | ||
| 3 | 1 | 1 | CA ACETATE | ||
| 4 | 1 | 2 | WATER | ||
| 5 | 1 | 2 | MPD |
