119D
CRYSTAL AND MOLECULAR STRUCTURE OF D(CGTAGATCTACG) AT 2.25 ANGSTROMS RESOLUTION
Experimental procedure
| Source type | SEALED TUBE |
| Temperature [K] | 288 |
| Detector technology | DIFFRACTOMETER |
| Detector | SYNTEX |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 64.840, 35.360, 25.350 |
| Unit cell angles | 90.00, 92.24, 90.00 |
Refinement procedure
| Resolution | 7.000 - 2.250 |
| R-factor | 0.138 |
| RMSD bond length | 0.026 |
| RMSD bond angle | 0.021 |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.200 |
| Rmerge | 0.040 * |
| Number of reflections | 3982 |
| Redundancy | 1.8 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 277 | pH 6.50, VAPOR DIFFUSION, SITTING DROP, temperature 277.00K |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | HEXANE-1,6-DIOL | ||
| 3 | 1 | 1 | NA CACODYLATE | ||
| 4 | 1 | 1 | MGCL2 | ||
| 5 | 1 | 1 | SPERMINE_HCL | ||
| 6 | 1 | 2 | WATER | ||
| 7 | 1 | 2 | HEXANE-1,6-DIOL |
