112M
SPERM WHALE MYOGLOBIN D122N N-PROPYL ISOCYANIDE AT PH 9.0
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | SIEMENS |
| Temperature [K] | 292 |
| Detector technology | IMAGE PLATE |
| Collection date | 1993-09 |
| Detector | RIGAKU |
| Spacegroup name | P 6 |
| Unit cell lengths | 91.420, 91.420, 45.580 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 5.000 - 2.340 |
| R-factor | 0.155 |
| Rwork | 0.155 |
| R-free | 0.23700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | SPERM WHALE MYOGLOBIN 0M D122N (DEOXY) |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.300 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | X-PLOR (3.851) |
| Refinement software | X-PLOR (3.851) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 6.000 | 2.350 |
| High resolution limit [Å] | 2.340 | 2.340 |
| Rmerge | 0.129 | 0.337 |
| Number of reflections | 8195 | |
| Completeness [%] | 87.6 | 91.3 |
| Redundancy | 4.89 | 4.47 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 9 | 3.0 M AMMONIUM SULFATE, 20 MM TRIS, 1MM EDTA, PH 9.0 |
