10HE

[3T-17,17,7-17N] Isosceles tensegrity triangle with 17, 17 and 7 base pairs between junctions and three turn edges

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-12-11
Detector	DECTRIS EIGER2 X 9M
Wavelength(s)	1.007430
Spacegroup name	P 1
Unit cell lengths	89.131, 99.497, 100.040
Unit cell angles	84.24, 64.20, 67.55

Refinement procedure

Resolution	46.370 - 6.330
R-factor	0.2171
Rwork	0.215
R-free	0.26670
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.705
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	91.668	7.732
High resolution limit [Å]	6.330	6.330
Number of reflections	2679	207
<I/σ(I)>	7.4
Completeness [%]	81.4
Redundancy	3.5
CC(1/2)	1.000	0.600

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	293	100 mM MOPS, 1.25 M magnesium sulfate