10HC
[17,17,7-7N_332] Isosceles tensegrity triangle with 17, 17 and 7 bp between junctions and 3, 3, and 2 turns of DNA per edge
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-12-11 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 1.007430 |
| Spacegroup name | P 1 |
| Unit cell lengths | 68.001, 86.145, 101.265 |
| Unit cell angles | 106.02, 102.27, 111.42 |
Refinement procedure
| Resolution | 48.020 - 5.490 |
| R-factor | 0.1686 |
| Rwork | 0.168 |
| R-free | 0.18820 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.814 |
| Data reduction software | autoPROC |
| Data scaling software | STARANISO |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 73.890 | 6.299 |
| High resolution limit [Å] | 5.485 | 5.485 |
| Number of reflections | 3362 | 198 |
| <I/σ(I)> | 7.7 | |
| Completeness [%] | 83.3 | |
| Redundancy | 3.6 | |
| CC(1/2) | 1.000 | 0.480 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 100 mM MOPS, 1.25 M magnesium sulfate |
