105M
SPERM WHALE MYOGLOBIN N-BUTYL ISOCYANIDE AT PH 9.0
Experimental procedure
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 292 |
Detector technology | IMAGE PLATE |
Collection date | 1993-07 |
Detector | RIGAKU |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 64.720, 30.061, 35.191 |
格子定数 [度] | 90.00, 105.76, 90.00 |
精密化法
残基 | 5.000 - 2.020 |
R因子 | 0.174 |
Rwork | 0.174 |
R-free | 0.26800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | SPERM WHALE MYOGLOBIN NBNC WITHOUT LIGAND |
結合長の平均二乗偏差(RMSD) [Å] | 0.007 |
結合角の平均二乗偏差(RMSD) [度] | 1.200 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | X-PLOR (3.851) |
Refinement software | X-PLOR (3.851) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 6.000 | 2.030 |
分解能 [Å] (高) | 2.020 | 2.020 |
Rmerge_l_obs | 0.071 | 0.225 |
独立反射数 | 7987 | |
完全性 [%] | 90.7 | 90.9 |
冗長性 | 1.82 | 1.96 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 9 | 3.0 M AMMONIUM SULFATE, UNBUFFERED, pH 9.0 |