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103M

SPERM WHALE MYOGLOBIN H64A N-BUTYL ISOCYANIDE AT PH 9.0

Experimental procedure
Source typeROTATING ANODE
Source detailsSIEMENS
Temperature [K]292
Detector technologyIMAGE PLATE
Collection date1996-10
DetectorRIGAKU
Spacegroup nameP 6
Unit cell lengths91.630, 91.630, 46.014
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution5.000 - 2.070
R-factor0.158
Rwork0.158
R-free0.21600
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)SPERM WHALE MYOGLOBIN 0M D122N (DEOXY)
RMSD bond length0.011
RMSD bond angle1.500
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareX-PLOR (3.851)
Refinement softwareX-PLOR (3.851)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]6.0002.080
High resolution limit [Å]2.0702.070
Rmerge0.0720.294
Number of reflections13413
Completeness [%]98.499.5
Redundancy5.175.24
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
193.0 M AMMONIUM SULFATE, 20 MM TRIS, 1MM EDTA, PH 9.0

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