マシュー密度: 2.28 Å3/Da / 溶媒含有率: 45.96 % 解説: MAD DATA AT 4 DIFFERENT WAVE LENGTHS WAS COLLECTED AT THE NSLS IN FEB-95 ON A CRYSTAL IN SPACE GROUP P 2 2 2 OF SELENOMETHIONYL-SUBSTITUTED PROTEIN. AN INITIAL STRUCTURE WAS DETERMINED FROM ...解説: MAD DATA AT 4 DIFFERENT WAVE LENGTHS WAS COLLECTED AT THE NSLS IN FEB-95 ON A CRYSTAL IN SPACE GROUP P 2 2 2 OF SELENOMETHIONYL-SUBSTITUTED PROTEIN. AN INITIAL STRUCTURE WAS DETERMINED FROM THIS MAD DATA AND USED AS A MOLECULAR REPLACEMENT SEARCH MODEL FOR THE DATA COLLECTED ON A NATIVE CRYSTAL IN SPACE GROUP C 2.
結晶化
pH: 5.2 / 詳細: pH 5.2
結晶化
*PLUS
温度: 100 K / 手法: 蒸気拡散法, ハンギングドロップ法
溶液の組成
*PLUS
ID
濃度
一般名
Crystal-ID
Sol-ID
化学式
1
5mM
1
drop
MnCl2
2
5mM
2-mercaptoethanol
1
drop
3
15mg/ml
protein
1
drop
4
14-20 %(w/v)
PEG3350
1
reservoir
5
100mM
1
reservoir
MnCl2
6
50mM
sodiumacetate
1
reservoir
-
データ収集
回折
平均測定温度: 100 K
放射光源
波長: 1.5418 Å
検出器
日付: 1994年9月1日
放射
散乱光タイプ: x-ray
放射波長
波長: 1.5418 Å / 相対比: 1
反射
解像度: 1.8→30 Å / Num. obs: 27543 / % possible obs: 76 % / Observed criterion σ(I): 0