温度: 293 K / 手法: 蒸気拡散法, ハンギングドロップ法 / pH: 4.7 詳細: Crystals grown at 0.17 M sodium citrate (pH 6) and 17-18% (w/v) PEG3350. Soaked for 1-2 minutes (empirically determined for each crystal) in equivalent solution with 0.025% (w/v) ...詳細: Crystals grown at 0.17 M sodium citrate (pH 6) and 17-18% (w/v) PEG3350. Soaked for 1-2 minutes (empirically determined for each crystal) in equivalent solution with 0.025% (w/v) glutaraldehyde. Finally transferred and soaked for 10-20 sec in solution containing 40% (w/v) PEG3350, 5 mM L-L-Asp, and 0.17 M sodium citrate (pH 4.7)
解像度: 2.3→26.5 Å / Cor.coef. Fo:Fc: 0.963 / Cor.coef. Fo:Fc free: 0.908 / SU B: 7.623 / SU ML: 0.184 / SU R Cruickshank DPI: 0.4248 / 交差検証法: THROUGHOUT / σ(F): 0 / ESU R: 0.425 / ESU R Free: 0.271 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS U VALUES : REFINED INDIVIDUALLY