PDB-4v5w: Grapevine Fanleaf virus

Basic information

• Entry: Database: PDB / ID: 4v5w
• Title: Grapevine Fanleaf virus
• Components: COAT PROTEIN
• Keywords: VIRUS / GFLV / FANLEAF DISEASE

Function / homology

Function:

transport of virus in host, cell to cell / host cell plasmodesma / viral capsid / host cell cytoplasm / host cell nucleus / structural molecule activity

Domain/homology:

Nepovirus subgroup A, RNA2 polyprotein, Protein 2A / Nepovirus subgroup A polyprotein / Nepovirus coat protein / Nepovirus coat protein, C-terminal / Nepovirus coat protein, N-terminal / Nepovirus coat protein, central domain / Nepovirus coat protein, C-terminal domain / Nepovirus coat protein, N-terminal domain / Viral coat protein subunit

Component:

RNA2 polyprotein

• Biological species: GRAPEVINE FANLEAF VIRUS
• Method: X-RAY DIFFRACTION / SYNCHROTRON / MOLECULAR REPLACEMENT / Resolution: 3.7 Å
• Authors: Schellenberger, P. / Demangeat, G. / Ritzenthaler, C. / Lorber, B. / Sauter, C.

Citation

Journal: Cryst.Growth Des. / Year: 2011
Title: Exploiting Protein Engineering and Crystal Polymorphism for Successful X-Ray Structure Determination
Authors: Bonnefond, L. / Schellenberger, P. / Basquin, J. / Demangeat, G. / Ritzenthaler, C. / Chenevert, R. / Balg, C. / Frugier, M. / Rudinger-Thirion, J. / Giege, R. / Lorber, B. / Sauter, C.

#1: Journal: J.Struct.Biol. / Year: 2011
Title: Strategies for the Crystallization of Viruses: Using Phase Diagrams and Gels to Produce 3D Crystals of Grapevine Fanleaf Virus.
Authors: Schellenberger, P. / Demangeat, G. / Lemaire, O. / Ritzenthaler, C. / Bergdoll, M. / Olieric, V. / Sauter, C. / Lorber, B.

History

Deposition	May 10, 2011	Deposition site: PDBE / Processing site: PDBE
Revision 1.0	Jul 9, 2014	Provider: repository / Type: Initial release
Supersession	Dec 10, 2014	ID: 2YI2, 2YI3, 2YI4
Revision 1.1	Dec 10, 2014	Group: Other
Revision 1.2	May 8, 2019	Group: Data collection / Experimental preparation / Other Category: exptl_crystal_grow / pdbx_database_proc / pdbx_database_status Item: _exptl_crystal_grow.method / _pdbx_database_status.date_author_approval / _pdbx_database_status.recvd_author_approval
Revision 1.3	Jan 10, 2024	Group: Data collection / Database references / Refinement description Category: chem_comp_atom / chem_comp_bond / database_2 / pdbx_initial_refinement_model Item: _database_2.pdbx_DOI / _database_2.pdbx_database_accession

Assembly

Deposited unit

AA: COAT PROTEIN

AB: COAT PROTEIN

AC: COAT PROTEIN

AD: COAT PROTEIN

AE: COAT PROTEIN

AF: COAT PROTEIN

AG: COAT PROTEIN

AH: COAT PROTEIN

AI: COAT PROTEIN

AJ: COAT PROTEIN

AK: COAT PROTEIN

AL: COAT PROTEIN

AM: COAT PROTEIN

AN: COAT PROTEIN

AO: COAT PROTEIN

AP: COAT PROTEIN

AQ: COAT PROTEIN

AR: COAT PROTEIN

AS: COAT PROTEIN

AT: COAT PROTEIN

BA: COAT PROTEIN

BB: COAT PROTEIN

BC: COAT PROTEIN

BD: COAT PROTEIN

BE: COAT PROTEIN

BF: COAT PROTEIN

BG: COAT PROTEIN

BH: COAT PROTEIN

BI: COAT PROTEIN

BJ: COAT PROTEIN

BK: COAT PROTEIN

BL: COAT PROTEIN

BM: COAT PROTEIN

BN: COAT PROTEIN

BO: COAT PROTEIN

BP: COAT PROTEIN

BQ: COAT PROTEIN

BR: COAT PROTEIN

BS: COAT PROTEIN

BT: COAT PROTEIN

CA: COAT PROTEIN

CB: COAT PROTEIN

CC: COAT PROTEIN

CD: COAT PROTEIN

CE: COAT PROTEIN

CF: COAT PROTEIN

CG: COAT PROTEIN

CH: COAT PROTEIN

CI: COAT PROTEIN

CJ: COAT PROTEIN

CK: COAT PROTEIN

CL: COAT PROTEIN

CM: COAT PROTEIN

CN: COAT PROTEIN

CO: COAT PROTEIN

CP: COAT PROTEIN

CQ: COAT PROTEIN

CR: COAT PROTEIN

CS: COAT PROTEIN

CT: COAT PROTEIN

Summary:

• 3.36 MDa, 60 polymers

Component details:

	Theoretical mass	Number of molelcules
Total (without water)	3,364,388	60
Polymers	3,364,388	60
Non-polymers	0	0
Water	0	0

1

Summary:

• Idetical with deposited unit
• defined by author&software

Symmetry operations:

Type	Name	Symmetry operation	Number
identity operation	1_555	x,y,z	1

Calculated values:

Method	PISA

Unit cell

Length a, b, c (Å)	283.600, 295.500, 394.300
Angle α, β, γ (deg.)	90.00, 91.60, 90.00
Int Tables number	4
Space group name H-M	P1211

Noncrystallographic symmetry (NCS)

NCS domain:

ID	Ens-ID
1	1
2	1
3	1
4	1
5	1
6	1
7	1
8	1
9	1
10	1
11	1
12	1
13	1
14	1
15	1
16	1
17	1
18	1
19	1
20	1
21	1
22	1
23	1
24	1
25	1
26	1
27	1
28	1
29	1
30	1
31	1
32	1
33	1
34	1
35	1
36	1
37	1
38	1
39	1
40	1
41	1
42	1
43	1
44	1
45	1
46	1
47	1
48	1
49	1
50	1
51	1
52	1
53	1
54	1
55	1
56	1
57	1
58	1
59	1
60	1
1	2
2	2
3	2
4	2
5	2
6	2
7	2
8	2
9	2
10	2
11	2
12	2
13	2
14	2
15	2
16	2
17	2
18	2
19	2
20	2
21	2
22	2
23	2
24	2
25	2
26	2
27	2
28	2
29	2
30	2
31	2
32	2
33	2
34	2
35	2
36	2
37	2
38	2
39	2
40	2
41	2
42	2
43	2
44	2
45	2
46	2
47	2
48	2
49	2
50	2
51	2
52	2
53	2
54	2
55	2
56	2
57	2
58	2
59	2
60	2
1	3
2	3
3	3
4	3
5	3
6	3
7	3
8	3
9	3
10	3
11	3
12	3
13	3
14	3
15	3
16	3
17	3
18	3
19	3
20	3
21	3
22	3
23	3
24	3
25	3
26	3
27	3
28	3
29	3
30	3
31	3
32	3
33	3
34	3
35	3
36	3
37	3
38	3
39	3
40	3
41	3
42	3
43	3
44	3
45	3
46	3
47	3
48	3
49	3
50	3
51	3
52	3
53	3
54	3
55	3
56	3
57	3
58	3
59	3
60	3
1	4
2	4
3	4
4	4
5	4
6	4
7	4
8	4
9	4
10	4
11	4
12	4
13	4
14	4
15	4
16	4
17	4
18	4
19	4
20	4
21	4
22	4
23	4
24	4
25	4
26	4
27	4
28	4
29	4
30	4
31	4
32	4
33	4
34	4
35	4
36	4
37	4
38	4
39	4
40	4
41	4
42	4
43	4
44	4
45	4
46	4
47	4
48	4
49	4
50	4
51	4
52	4
53	4
54	4
55	4
56	4
57	4
58	4
59	4
60	4

NCS domain segments:

Dom-ID	Component-ID	Ens-ID	Selection details
1	1	1	(CHAIN AA AND RESID 1:8)
2	1	1	(CHAIN AB AND RESID 1:8)
3	1	1	(CHAIN AC AND RESID 1:8)
4	1	1	(CHAIN AD AND RESID 1:8)
5	1	1	(CHAIN AE AND RESID 1:8)
6	1	1	(CHAIN AF AND RESID 1:8)
7	1	1	(CHAIN AG AND RESID 1:8)
8	1	1	(CHAIN AH AND RESID 1:8)
9	1	1	(CHAIN AI AND RESID 1:8)
10	1	1	(CHAIN AJ AND RESID 1:8)
11	1	1	(CHAIN AK AND RESID 1:8)
12	1	1	(CHAIN AL AND RESID 1:8)
13	1	1	(CHAIN AM AND RESID 1:8)
14	1	1	(CHAIN AN AND RESID 1:8)
15	1	1	(CHAIN AO AND RESID 1:8)
16	1	1	(CHAIN AP AND RESID 1:8)
17	1	1	(CHAIN AQ AND RESID 1:8)
18	1	1	(CHAIN AR AND RESID 1:8)
19	1	1	(CHAIN AS AND RESID 1:8)
20	1	1	(CHAIN AT AND RESID 1:8)
21	1	1	(CHAIN BA AND RESID 1:8)
22	1	1	(CHAIN BB AND RESID 1:8)
23	1	1	(CHAIN BC AND RESID 1:8)
24	1	1	(CHAIN BD AND RESID 1:8)
25	1	1	(CHAIN BE AND RESID 1:8)
26	1	1	(CHAIN BF AND RESID 1:8)
27	1	1	(CHAIN BG AND RESID 1:8)
28	1	1	(CHAIN BH AND RESID 1:8)
29	1	1	(CHAIN BI AND RESID 1:8)
30	1	1	(CHAIN BJ AND RESID 1:8)
31	1	1	(CHAIN BK AND RESID 1:8)
32	1	1	(CHAIN BL AND RESID 1:8)
33	1	1	(CHAIN BM AND RESID 1:8)
34	1	1	(CHAIN BN AND RESID 1:8)
35	1	1	(CHAIN BO AND RESID 1:8)
36	1	1	(CHAIN BP AND RESID 1:8)
37	1	1	(CHAIN BQ AND RESID 1:8)
38	1	1	(CHAIN BR AND RESID 1:8)
39	1	1	(CHAIN BS AND RESID 1:8)
40	1	1	(CHAIN BT AND RESID 1:8)
41	1	1	(CHAIN CA AND RESID 1:8)
42	1	1	(CHAIN CB AND RESID 1:8)
43	1	1	(CHAIN CC AND RESID 1:8)
44	1	1	(CHAIN CD AND RESID 1:8)
45	1	1	(CHAIN CE AND RESID 1:8)
46	1	1	(CHAIN CF AND RESID 1:8)
47	1	1	(CHAIN CG AND RESID 1:8)
48	1	1	(CHAIN CH AND RESID 1:8)
49	1	1	(CHAIN CI AND RESID 1:8)
50	1	1	(CHAIN CJ AND RESID 1:8)
51	1	1	(CHAIN CK AND RESID 1:8)
52	1	1	(CHAIN CL AND RESID 1:8)
53	1	1	(CHAIN CM AND RESID 1:8)
54	1	1	(CHAIN CN AND RESID 1:8)
55	1	1	(CHAIN CO AND RESID 1:8)
56	1	1	(CHAIN CP AND RESID 1:8)
57	1	1	(CHAIN CQ AND RESID 1:8)
58	1	1	(CHAIN CR AND RESID 1:8)
59	1	1	(CHAIN CS AND RESID 1:8)
60	1	1	(CHAIN CT AND RESID 1:8)
1	1	2	(CHAIN AA AND RESID 20:74)
2	1	2	(CHAIN AB AND RESID 20:74)
3	1	2	(CHAIN AC AND RESID 20:74)
4	1	2	(CHAIN AD AND RESID 20:74)
5	1	2	(CHAIN AE AND RESID 20:74)
6	1	2	(CHAIN AF AND RESID 20:74)
7	1	2	(CHAIN AG AND RESID 20:74)
8	1	2	(CHAIN AH AND RESID 20:74)
9	1	2	(CHAIN AI AND RESID 20:74)
10	1	2	(CHAIN AJ AND RESID 20:74)
11	1	2	(CHAIN AK AND RESID 20:74)
12	1	2	(CHAIN AL AND RESID 20:74)
13	1	2	(CHAIN AM AND RESID 20:74)
14	1	2	(CHAIN AN AND RESID 20:74)
15	1	2	(CHAIN AO AND RESID 20:74)
16	1	2	(CHAIN AP AND RESID 20:74)
17	1	2	(CHAIN AQ AND RESID 20:74)
18	1	2	(CHAIN AR AND RESID 20:74)
19	1	2	(CHAIN AS AND RESID 20:74)
20	1	2	(CHAIN AT AND RESID 20:74)
21	1	2	(CHAIN BA AND RESID 20:74)
22	1	2	(CHAIN BB AND RESID 20:74)
23	1	2	(CHAIN BC AND RESID 20:74)
24	1	2	(CHAIN BD AND RESID 20:74)
25	1	2	(CHAIN BE AND RESID 20:74)
26	1	2	(CHAIN BF AND RESID 20:74)
27	1	2	(CHAIN BG AND RESID 20:74)
28	1	2	(CHAIN BH AND RESID 20:74)
29	1	2	(CHAIN BI AND RESID 20:74)
30	1	2	(CHAIN BJ AND RESID 20:74)
31	1	2	(CHAIN BK AND RESID 20:74)
32	1	2	(CHAIN BL AND RESID 20:74)
33	1	2	(CHAIN BM AND RESID 20:74)
34	1	2	(CHAIN BN AND RESID 20:74)
35	1	2	(CHAIN BO AND RESID 20:74)
36	1	2	(CHAIN BP AND RESID 20:74)
37	1	2	(CHAIN BQ AND RESID 20:74)
38	1	2	(CHAIN BR AND RESID 20:74)
39	1	2	(CHAIN BS AND RESID 20:74)
40	1	2	(CHAIN BT AND RESID 20:74)
41	1	2	(CHAIN CA AND RESID 20:74)
42	1	2	(CHAIN CB AND RESID 20:74)
43	1	2	(CHAIN CC AND RESID 20:74)
44	1	2	(CHAIN CD AND RESID 20:74)
45	1	2	(CHAIN CE AND RESID 20:74)
46	1	2	(CHAIN CF AND RESID 20:74)
47	1	2	(CHAIN CG AND RESID 20:74)
48	1	2	(CHAIN CH AND RESID 20:74)
49	1	2	(CHAIN CI AND RESID 20:74)
50	1	2	(CHAIN CJ AND RESID 20:74)
51	1	2	(CHAIN CK AND RESID 20:74)
52	1	2	(CHAIN CL AND RESID 20:74)
53	1	2	(CHAIN CM AND RESID 20:74)
54	1	2	(CHAIN CN AND RESID 20:74)
55	1	2	(CHAIN CO AND RESID 20:74)
56	1	2	(CHAIN CP AND RESID 20:74)
57	1	2	(CHAIN CQ AND RESID 20:74)
58	1	2	(CHAIN CR AND RESID 20:74)
59	1	2	(CHAIN CS AND RESID 20:74)
60	1	2	(CHAIN CT AND RESID 20:74)
1	1	3	(CHAIN AA AND RESID 86:294)
2	1	3	(CHAIN AB AND RESID 86:294)
3	1	3	(CHAIN AC AND RESID 86:294)
4	1	3	(CHAIN AD AND RESID 86:294)
5	1	3	(CHAIN AE AND RESID 86:294)
6	1	3	(CHAIN AF AND RESID 86:294)
7	1	3	(CHAIN AG AND RESID 86:294)
8	1	3	(CHAIN AH AND RESID 86:294)
9	1	3	(CHAIN AI AND RESID 86:294)
10	1	3	(CHAIN AJ AND RESID 86:294)
11	1	3	(CHAIN AK AND RESID 86:294)
12	1	3	(CHAIN AL AND RESID 86:294)
13	1	3	(CHAIN AM AND RESID 86:294)
14	1	3	(CHAIN AN AND RESID 86:294)
15	1	3	(CHAIN AO AND RESID 86:294)
16	1	3	(CHAIN AP AND RESID 86:294)
17	1	3	(CHAIN AQ AND RESID 86:294)
18	1	3	(CHAIN AR AND RESID 86:294)
19	1	3	(CHAIN AS AND RESID 86:294)
20	1	3	(CHAIN AT AND RESID 86:294)
21	1	3	(CHAIN BA AND RESID 86:294)
22	1	3	(CHAIN BB AND RESID 86:294)
23	1	3	(CHAIN BC AND RESID 86:294)
24	1	3	(CHAIN BD AND RESID 86:294)
25	1	3	(CHAIN BE AND RESID 86:294)
26	1	3	(CHAIN BF AND RESID 86:294)
27	1	3	(CHAIN BG AND RESID 86:294)
28	1	3	(CHAIN BH AND RESID 86:294)
29	1	3	(CHAIN BI AND RESID 86:294)
30	1	3	(CHAIN BJ AND RESID 86:294)
31	1	3	(CHAIN BK AND RESID 86:294)
32	1	3	(CHAIN BL AND RESID 86:294)
33	1	3	(CHAIN BM AND RESID 86:294)
34	1	3	(CHAIN BN AND RESID 86:294)
35	1	3	(CHAIN BO AND RESID 86:294)
36	1	3	(CHAIN BP AND RESID 86:294)
37	1	3	(CHAIN BQ AND RESID 86:294)
38	1	3	(CHAIN BR AND RESID 86:294)
39	1	3	(CHAIN BS AND RESID 86:294)
40	1	3	(CHAIN BT AND RESID 86:294)
41	1	3	(CHAIN CA AND RESID 86:294)
42	1	3	(CHAIN CB AND RESID 86:294)
43	1	3	(CHAIN CC AND RESID 86:294)
44	1	3	(CHAIN CD AND RESID 86:294)
45	1	3	(CHAIN CE AND RESID 86:294)
46	1	3	(CHAIN CF AND RESID 86:294)
47	1	3	(CHAIN CG AND RESID 86:294)
48	1	3	(CHAIN CH AND RESID 86:294)
49	1	3	(CHAIN CI AND RESID 86:294)
50	1	3	(CHAIN CJ AND RESID 86:294)
51	1	3	(CHAIN CK AND RESID 86:294)
52	1	3	(CHAIN CL AND RESID 86:294)
53	1	3	(CHAIN CM AND RESID 86:294)
54	1	3	(CHAIN CN AND RESID 86:294)
55	1	3	(CHAIN CO AND RESID 86:294)
56	1	3	(CHAIN CP AND RESID 86:294)
57	1	3	(CHAIN CQ AND RESID 86:294)
58	1	3	(CHAIN CR AND RESID 86:294)
59	1	3	(CHAIN CS AND RESID 86:294)
60	1	3	(CHAIN CT AND RESID 86:294)
1	1	4	(CHAIN AA AND RESID 303:504)
2	1	4	(CHAIN AB AND RESID 303:504)
3	1	4	(CHAIN AC AND RESID 303:504)
4	1	4	(CHAIN AD AND RESID 303:504)
5	1	4	(CHAIN AE AND RESID 303:504)
6	1	4	(CHAIN AF AND RESID 303:504)
7	1	4	(CHAIN AG AND RESID 303:504)
8	1	4	(CHAIN AH AND RESID 303:504)
9	1	4	(CHAIN AI AND RESID 303:504)
10	1	4	(CHAIN AJ AND RESID 303:504)
11	1	4	(CHAIN AK AND RESID 303:504)
12	1	4	(CHAIN AL AND RESID 303:504)
13	1	4	(CHAIN AM AND RESID 303:504)
14	1	4	(CHAIN AN AND RESID 303:504)
15	1	4	(CHAIN AO AND RESID 303:504)
16	1	4	(CHAIN AP AND RESID 303:504)
17	1	4	(CHAIN AQ AND RESID 303:504)
18	1	4	(CHAIN AR AND RESID 303:504)
19	1	4	(CHAIN AS AND RESID 303:504)
20	1	4	(CHAIN AT AND RESID 303:504)
21	1	4	(CHAIN BA AND RESID 303:504)
22	1	4	(CHAIN BB AND RESID 303:504)
23	1	4	(CHAIN BC AND RESID 303:504)
24	1	4	(CHAIN BD AND RESID 303:504)
25	1	4	(CHAIN BE AND RESID 303:504)
26	1	4	(CHAIN BF AND RESID 303:504)
27	1	4	(CHAIN BG AND RESID 303:504)
28	1	4	(CHAIN BH AND RESID 303:504)
29	1	4	(CHAIN BI AND RESID 303:504)
30	1	4	(CHAIN BJ AND RESID 303:504)
31	1	4	(CHAIN BK AND RESID 303:504)
32	1	4	(CHAIN BL AND RESID 303:504)
33	1	4	(CHAIN BM AND RESID 303:504)
34	1	4	(CHAIN BN AND RESID 303:504)
35	1	4	(CHAIN BO AND RESID 303:504)
36	1	4	(CHAIN BP AND RESID 303:504)
37	1	4	(CHAIN BQ AND RESID 303:504)
38	1	4	(CHAIN BR AND RESID 303:504)
39	1	4	(CHAIN BS AND RESID 303:504)
40	1	4	(CHAIN BT AND RESID 303:504)
41	1	4	(CHAIN CA AND RESID 303:504)
42	1	4	(CHAIN CB AND RESID 303:504)
43	1	4	(CHAIN CC AND RESID 303:504)
44	1	4	(CHAIN CD AND RESID 303:504)
45	1	4	(CHAIN CE AND RESID 303:504)
46	1	4	(CHAIN CF AND RESID 303:504)
47	1	4	(CHAIN CG AND RESID 303:504)
48	1	4	(CHAIN CH AND RESID 303:504)
49	1	4	(CHAIN CI AND RESID 303:504)
50	1	4	(CHAIN CJ AND RESID 303:504)
51	1	4	(CHAIN CK AND RESID 303:504)
52	1	4	(CHAIN CL AND RESID 303:504)
53	1	4	(CHAIN CM AND RESID 303:504)
54	1	4	(CHAIN CN AND RESID 303:504)
55	1	4	(CHAIN CO AND RESID 303:504)
56	1	4	(CHAIN CP AND RESID 303:504)
57	1	4	(CHAIN CQ AND RESID 303:504)
58	1	4	(CHAIN CR AND RESID 303:504)
59	1	4	(CHAIN CS AND RESID 303:504)
60	1	4	(CHAIN CT AND RESID 303:504)

NCS ensembles :

ID
1
2
3
4

Components

#1: Protein

AA AB AC AD AE AF AG AH AI AJ AK AL AM AN AO AP AQ AR AS ...
COAT PROTEIN / 2C-CP

Details:

Mass: 56073.141 Da / Num. of mol.: 60 / Source method: isolated from a natural source / Source: (natural) GRAPEVINE FANLEAF VIRUS / Strain: GFLV-F13 / References: UniProt: P18474

Experimental details

Experiment

• Experiment: Method: X-RAY DIFFRACTION / Number of used crystals: 2

Sample preparation

• Crystal: Density Matthews: 4.9 ų/Da / Density % sol: 75 % / Description: NONE
• Crystal grow: Method: vapor diffusion, sitting drop / pH: 7.5 ; Details: SITTING DROP (VAPOR DIFFUSION) COMPOSED OF 1:1 MIXTURE OF 1.5 MG/ML GFLV SOLUTION AND OF THE RESERVOIR SOLUTION: 3.75% (M/V) PEG3350, 0.1M NA-HEPES PH 7.5, 0.2% (M/V) AGAROSE GEL.

Data collection

• Diffraction: Mean temperature: 100 K
• Diffraction source: Source: SYNCHROTRON / Site: SLS / Beamline: X06DA / Wavelength: 0.9794
• Detector: Type: MARMOSAIC 225 mm CCD / Detector: CCD / Date: Mar 27, 2009
• Radiation: Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
• Radiation wavelength: Wavelength: 0.9794 Å / Relative weight: 1
• Reflection: Resolution: 3.7→50 Å / Num. obs: 682148 / % possible obs: 99 % / Observed criterion σ(I): -3 / Redundancy: 6.2 % / B_iso Wilson estimate: 66.08 Ų / R_merge(I) obs: 0.27 / Net I/σ(I): 8.4
• Reflection shell: Resolution: 3.7→3.8 Å / Redundancy: 2.9 % / R_merge(I) obs: 0.58 / Mean I/σ(I) obs: 2 / % possible all: 87.6

Processing

Software

Name	Version	Classification
AMoRE		model building
PHENIX	(PHENIX.REFINE)	refinement
XDS		data reduction
XSCALE		data scaling
AMoRE		phasing

Refinement

Method to determine structure: MOLECULAR REPLACEMENT
Starting model: PDB ENTRY 2Y26

2y26

Resolution: 3.7→49.799 Å / SU ML: 0.42 / σ(F): 1.34 / Phase error: 22.71 / Stereochemistry target values: ML
Details: THE PROTEIN CONTENT OF THIS CRYSTAL WAS 0.25 OF THE UNIT CELL WHICH CORRESPONDS TO A VM OF 5. WHEN THE VIRAL CAVITY THAT CONTAINS THE GENOMIC RNA IS EXCLUDED, THE ACTUAL FRACTION OF UNIT CELL OCCUPIED BY SOLVENT IS ABOUT 0.24. IN THE

	Rfactor	Num. reflection	% reflection
Rfree	0.2469	34195	5 %
Rwork	0.2315	-	-
obs	0.2323	682148	99 %

• Solvent computation: Shrinkage radii: 0.83 Å / VDW probe radii: 1.1 Å / Solvent model: FLAT BULK SOLVENT MODEL / B_sol: 31.912 Ų / k_sol: 0.316 e/ų

Displacement parameters

	Baniso -1	Baniso -2	Baniso -3
1-	-7.406 Å2	0 Å2	8.8842 Å2
2-	-	-12.4026 Å2	0 Å2
3-	-	-	19.8085 Å2

Refinement step

Cycle: LAST / Resolution: 3.7→49.799 Å

	Protein	Nucleic acid	Ligand	Solvent	Total
Num. atoms	79020	0	0	0	79020

Refine LS restraints

Refine-ID	Type	Dev ideal	Number
X-RAY DIFFRACTION	f_bond_d	0.01	100000
X-RAY DIFFRACTION	f_angle_d	1.201	100000
X-RAY DIFFRACTION	f_dihedral_angle_d	14.541	86520
X-RAY DIFFRACTION	f_chiral_restr	0.077	36900
X-RAY DIFFRACTION	f_plane_restr	0.005	42060

Refine LS restraints NCS

Ens-ID	Dom-ID	Auth asym-ID	Number	Refine-ID	Type	Rms dev position (Å)
1	1	AA	51	X-RAY DIFFRACTION	POSITIONAL
1	2	AB	51	X-RAY DIFFRACTION	POSITIONAL	0.032
1	3	AC	51	X-RAY DIFFRACTION	POSITIONAL	0.039
1	4	AD	51	X-RAY DIFFRACTION	POSITIONAL	0.035
1	5	AE	51	X-RAY DIFFRACTION	POSITIONAL	0.04
1	6	AF	51	X-RAY DIFFRACTION	POSITIONAL	0.038
1	7	AG	51	X-RAY DIFFRACTION	POSITIONAL	0.043
1	8	AH	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	9	AI	51	X-RAY DIFFRACTION	POSITIONAL	0.045
1	10	AJ	51	X-RAY DIFFRACTION	POSITIONAL	0.036
1	11	AK	51	X-RAY DIFFRACTION	POSITIONAL	0.04
1	12	AL	51	X-RAY DIFFRACTION	POSITIONAL	0.036
1	13	AM	51	X-RAY DIFFRACTION	POSITIONAL	0.04
1	14	AN	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	15	AO	51	X-RAY DIFFRACTION	POSITIONAL	0.031
1	16	AP	51	X-RAY DIFFRACTION	POSITIONAL	0.044
1	17	AQ	51	X-RAY DIFFRACTION	POSITIONAL	0.036
1	18	AR	51	X-RAY DIFFRACTION	POSITIONAL	0.039
1	19	AS	51	X-RAY DIFFRACTION	POSITIONAL	0.038
1	20	AT	51	X-RAY DIFFRACTION	POSITIONAL	0.04
1	21	BA	51	X-RAY DIFFRACTION	POSITIONAL	0.039
1	22	BB	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	23	BC	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	24	BD	51	X-RAY DIFFRACTION	POSITIONAL	0.035
1	25	BE	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	26	BF	51	X-RAY DIFFRACTION	POSITIONAL	0.038
1	27	BG	51	X-RAY DIFFRACTION	POSITIONAL	0.04
1	28	BH	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	29	BI	51	X-RAY DIFFRACTION	POSITIONAL	0.034
1	30	BJ	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	31	BK	51	X-RAY DIFFRACTION	POSITIONAL	0.041
1	32	BL	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	33	BM	51	X-RAY DIFFRACTION	POSITIONAL	0.044
1	34	BN	51	X-RAY DIFFRACTION	POSITIONAL	0.043
1	35	BO	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	36	BP	51	X-RAY DIFFRACTION	POSITIONAL	0.053
1	37	BQ	51	X-RAY DIFFRACTION	POSITIONAL	0.039
1	38	BR	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	39	BS	51	X-RAY DIFFRACTION	POSITIONAL	0.038
1	40	BT	51	X-RAY DIFFRACTION	POSITIONAL	0.036
1	41	CA	51	X-RAY DIFFRACTION	POSITIONAL	0.039
1	42	CB	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	43	CC	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	44	CD	51	X-RAY DIFFRACTION	POSITIONAL	0.035
1	45	CE	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	46	CF	51	X-RAY DIFFRACTION	POSITIONAL	0.04
1	47	CG	51	X-RAY DIFFRACTION	POSITIONAL	0.038
1	48	CH	51	X-RAY DIFFRACTION	POSITIONAL	0.033
1	49	CI	51	X-RAY DIFFRACTION	POSITIONAL	0.038
1	50	CJ	51	X-RAY DIFFRACTION	POSITIONAL	0.043
1	51	CK	51	X-RAY DIFFRACTION	POSITIONAL	0.037
1	52	CL	51	X-RAY DIFFRACTION	POSITIONAL	0.051
1	53	CM	51	X-RAY DIFFRACTION	POSITIONAL	0.041
1	54	CN	51	X-RAY DIFFRACTION	POSITIONAL	0.043
1	55	CO	51	X-RAY DIFFRACTION	POSITIONAL	0.038
1	56	CP	51	X-RAY DIFFRACTION	POSITIONAL	0.041
1	57	CQ	51	X-RAY DIFFRACTION	POSITIONAL	0.042
1	58	CR	51	X-RAY DIFFRACTION	POSITIONAL	0.041
1	59	CS	51	X-RAY DIFFRACTION	POSITIONAL	0.034
1	60	CT	51	X-RAY DIFFRACTION	POSITIONAL	0.037
2	1	AA	440	X-RAY DIFFRACTION	POSITIONAL
2	2	AB	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	3	AC	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	4	AD	440	X-RAY DIFFRACTION	POSITIONAL	0.037
2	5	AE	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	6	AF	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	7	AG	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	8	AH	440	X-RAY DIFFRACTION	POSITIONAL	0.042
2	9	AI	440	X-RAY DIFFRACTION	POSITIONAL	0.038
2	10	AJ	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	11	AK	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	12	AL	440	X-RAY DIFFRACTION	POSITIONAL	0.042
2	13	AM	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	14	AN	440	X-RAY DIFFRACTION	POSITIONAL	0.041
2	15	AO	440	X-RAY DIFFRACTION	POSITIONAL	0.041
2	16	AP	440	X-RAY DIFFRACTION	POSITIONAL	0.043
2	17	AQ	440	X-RAY DIFFRACTION	POSITIONAL	0.041
2	18	AR	440	X-RAY DIFFRACTION	POSITIONAL	0.041
2	19	AS	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	20	AT	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	21	BA	440	X-RAY DIFFRACTION	POSITIONAL	0.038
2	22	BB	440	X-RAY DIFFRACTION	POSITIONAL	0.042
2	23	BC	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	24	BD	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	25	BE	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	26	BF	440	X-RAY DIFFRACTION	POSITIONAL	0.044
2	27	BG	440	X-RAY DIFFRACTION	POSITIONAL	0.038
2	28	BH	440	X-RAY DIFFRACTION	POSITIONAL	0.041
2	29	BI	440	X-RAY DIFFRACTION	POSITIONAL	0.042
2	30	BJ	440	X-RAY DIFFRACTION	POSITIONAL	0.038
2	31	BK	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	32	BL	440	X-RAY DIFFRACTION	POSITIONAL	0.042
2	33	BM	440	X-RAY DIFFRACTION	POSITIONAL	0.041
2	34	BN	440	X-RAY DIFFRACTION	POSITIONAL	0.042
2	35	BO	440	X-RAY DIFFRACTION	POSITIONAL	0.038
2	36	BP	440	X-RAY DIFFRACTION	POSITIONAL	0.044
2	37	BQ	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	38	BR	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	39	BS	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	40	BT	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	41	CA	440	X-RAY DIFFRACTION	POSITIONAL	0.043
2	42	CB	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	43	CC	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	44	CD	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	45	CE	440	X-RAY DIFFRACTION	POSITIONAL	0.037
2	46	CF	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	47	CG	440	X-RAY DIFFRACTION	POSITIONAL	0.044
2	48	CH	440	X-RAY DIFFRACTION	POSITIONAL	0.042
2	49	CI	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	50	CJ	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	51	CK	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	52	CL	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	53	CM	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	54	CN	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	55	CO	440	X-RAY DIFFRACTION	POSITIONAL	0.04
2	56	CP	440	X-RAY DIFFRACTION	POSITIONAL	0.042
2	57	CQ	440	X-RAY DIFFRACTION	POSITIONAL	0.039
2	58	CR	440	X-RAY DIFFRACTION	POSITIONAL	0.043
2	59	CS	440	X-RAY DIFFRACTION	POSITIONAL	0.038
2	60	CT	440	X-RAY DIFFRACTION	POSITIONAL	0.041
3	1	AA	1653	X-RAY DIFFRACTION	POSITIONAL
3	2	AB	1653	X-RAY DIFFRACTION	POSITIONAL	0.211
3	3	AC	1653	X-RAY DIFFRACTION	POSITIONAL	0.038
3	4	AD	1653	X-RAY DIFFRACTION	POSITIONAL	0.036
3	5	AE	1653	X-RAY DIFFRACTION	POSITIONAL	0.042
3	6	AF	1653	X-RAY DIFFRACTION	POSITIONAL	0.036
3	7	AG	1653	X-RAY DIFFRACTION	POSITIONAL	0.29
3	8	AH	1653	X-RAY DIFFRACTION	POSITIONAL	0.041
3	9	AI	1653	X-RAY DIFFRACTION	POSITIONAL	0.041
3	10	AJ	1653	X-RAY DIFFRACTION	POSITIONAL	0.139
3	11	AK	1653	X-RAY DIFFRACTION	POSITIONAL	0.038
3	12	AL	1653	X-RAY DIFFRACTION	POSITIONAL	0.039
3	13	AM	1653	X-RAY DIFFRACTION	POSITIONAL	0.04
3	14	AN	1653	X-RAY DIFFRACTION	POSITIONAL	0.041
3	15	AO	1653	X-RAY DIFFRACTION	POSITIONAL	0.128
3	16	AP	1653	X-RAY DIFFRACTION	POSITIONAL	0.044
3	17	AQ	1653	X-RAY DIFFRACTION	POSITIONAL	0.038
3	18	AR	1653	X-RAY DIFFRACTION	POSITIONAL	0.045
3	19	AS	1653	X-RAY DIFFRACTION	POSITIONAL	0.043
3	20	AT	1653	X-RAY DIFFRACTION	POSITIONAL	0.038
3	21	BA	1653	X-RAY DIFFRACTION	POSITIONAL	0.037
3	22	BB	1653	X-RAY DIFFRACTION	POSITIONAL	0.043
3	23	BC	1653	X-RAY DIFFRACTION	POSITIONAL	0.037
3	24	BD	1653	X-RAY DIFFRACTION	POSITIONAL	0.038
3	25	BE	1653	X-RAY DIFFRACTION	POSITIONAL	0.04
3	26	BF	1653	X-RAY DIFFRACTION	POSITIONAL	0.041
3	27	BG	1653	X-RAY DIFFRACTION	POSITIONAL	0.039
3	28	BH	1653	X-RAY DIFFRACTION	POSITIONAL	0.04
3	29	BI	1653	X-RAY DIFFRACTION	POSITIONAL	0.041
3	30	BJ	1653	X-RAY DIFFRACTION	POSITIONAL	0.043
3	31	BK	1653	X-RAY DIFFRACTION	POSITIONAL	0.038
3	32	BL	1653	X-RAY DIFFRACTION	POSITIONAL	0.04
3	33	BM	1653	X-RAY DIFFRACTION	POSITIONAL	0.043
3	34	BN	1653	X-RAY DIFFRACTION	POSITIONAL	0.041
3	35	BO	1653	X-RAY DIFFRACTION	POSITIONAL	0.042
3	36	BP	1653	X-RAY DIFFRACTION	POSITIONAL	0.05
3	37	BQ	1653	X-RAY DIFFRACTION	POSITIONAL	0.039
3	38	BR	1653	X-RAY DIFFRACTION	POSITIONAL	0.039
3	39	BS	1653	X-RAY DIFFRACTION	POSITIONAL	0.039
3	40	BT	1653	X-RAY DIFFRACTION	POSITIONAL	0.038
3	41	CA	1653	X-RAY DIFFRACTION	POSITIONAL	0.039
3	42	CB	1653	X-RAY DIFFRACTION	POSITIONAL	0.039
3	43	CC	1653	X-RAY DIFFRACTION	POSITIONAL	0.043
3	44	CD	1653	X-RAY DIFFRACTION	POSITIONAL	0.038
3	45	CE	1653	X-RAY DIFFRACTION	POSITIONAL	0.04
3	46	CF	1653	X-RAY DIFFRACTION	POSITIONAL	0.04
3	47	CG	1653	X-RAY DIFFRACTION	POSITIONAL	0.047
3	48	CH	1653	X-RAY DIFFRACTION	POSITIONAL	0.041
3	49	CI	1653	X-RAY DIFFRACTION	POSITIONAL	0.041
3	50	CJ	1653	X-RAY DIFFRACTION	POSITIONAL	0.041
3	51	CK	1653	X-RAY DIFFRACTION	POSITIONAL	0.039
3	52	CL	1653	X-RAY DIFFRACTION	POSITIONAL	0.038
3	53	CM	1653	X-RAY DIFFRACTION	POSITIONAL	0.043
3	54	CN	1653	X-RAY DIFFRACTION	POSITIONAL	0.04
3	55	CO	1653	X-RAY DIFFRACTION	POSITIONAL	0.045
3	56	CP	1653	X-RAY DIFFRACTION	POSITIONAL	0.04
3	57	CQ	1653	X-RAY DIFFRACTION	POSITIONAL	0.037
3	58	CR	1653	X-RAY DIFFRACTION	POSITIONAL	0.082
3	59	CS	1653	X-RAY DIFFRACTION	POSITIONAL	0.039
3	60	CT	1653	X-RAY DIFFRACTION	POSITIONAL	0.038
4	1	AA	1570	X-RAY DIFFRACTION	POSITIONAL
4	2	AB	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	3	AC	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	4	AD	1570	X-RAY DIFFRACTION	POSITIONAL	0.043
4	5	AE	1570	X-RAY DIFFRACTION	POSITIONAL	0.043
4	6	AF	1570	X-RAY DIFFRACTION	POSITIONAL	0.039
4	7	AG	1570	X-RAY DIFFRACTION	POSITIONAL	0.04
4	8	AH	1570	X-RAY DIFFRACTION	POSITIONAL	0.04
4	9	AI	1570	X-RAY DIFFRACTION	POSITIONAL	0.044
4	10	AJ	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	11	AK	1570	X-RAY DIFFRACTION	POSITIONAL	0.043
4	12	AL	1570	X-RAY DIFFRACTION	POSITIONAL	0.176
4	13	AM	1570	X-RAY DIFFRACTION	POSITIONAL	0.207
4	14	AN	1570	X-RAY DIFFRACTION	POSITIONAL	0.044
4	15	AO	1570	X-RAY DIFFRACTION	POSITIONAL	0.043
4	16	AP	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	17	AQ	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	18	AR	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	19	AS	1570	X-RAY DIFFRACTION	POSITIONAL	0.039
4	20	AT	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	21	BA	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	22	BB	1570	X-RAY DIFFRACTION	POSITIONAL	0.049
4	23	BC	1570	X-RAY DIFFRACTION	POSITIONAL	0.039
4	24	BD	1570	X-RAY DIFFRACTION	POSITIONAL	0.152
4	25	BE	1570	X-RAY DIFFRACTION	POSITIONAL	0.04
4	26	BF	1570	X-RAY DIFFRACTION	POSITIONAL	0.042
4	27	BG	1570	X-RAY DIFFRACTION	POSITIONAL	0.043
4	28	BH	1570	X-RAY DIFFRACTION	POSITIONAL	0.042
4	29	BI	1570	X-RAY DIFFRACTION	POSITIONAL	0.044
4	30	BJ	1570	X-RAY DIFFRACTION	POSITIONAL	0.04
4	31	BK	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	32	BL	1570	X-RAY DIFFRACTION	POSITIONAL	0.044
4	33	BM	1570	X-RAY DIFFRACTION	POSITIONAL	0.043
4	34	BN	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	35	BO	1570	X-RAY DIFFRACTION	POSITIONAL	0.043
4	36	BP	1570	X-RAY DIFFRACTION	POSITIONAL	0.043
4	37	BQ	1570	X-RAY DIFFRACTION	POSITIONAL	0.04
4	38	BR	1570	X-RAY DIFFRACTION	POSITIONAL	0.042
4	39	BS	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	40	BT	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	41	CA	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	42	CB	1570	X-RAY DIFFRACTION	POSITIONAL	0.04
4	43	CC	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	44	CD	1570	X-RAY DIFFRACTION	POSITIONAL	0.04
4	45	CE	1570	X-RAY DIFFRACTION	POSITIONAL	0.04
4	46	CF	1570	X-RAY DIFFRACTION	POSITIONAL	0.04
4	47	CG	1570	X-RAY DIFFRACTION	POSITIONAL	0.044
4	48	CH	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	49	CI	1570	X-RAY DIFFRACTION	POSITIONAL	0.257
4	50	CJ	1570	X-RAY DIFFRACTION	POSITIONAL	0.042
4	51	CK	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	52	CL	1570	X-RAY DIFFRACTION	POSITIONAL	0.042
4	53	CM	1570	X-RAY DIFFRACTION	POSITIONAL	0.041
4	54	CN	1570	X-RAY DIFFRACTION	POSITIONAL	0.042
4	55	CO	1570	X-RAY DIFFRACTION	POSITIONAL	0.04
4	56	CP	1570	X-RAY DIFFRACTION	POSITIONAL	0.043
4	57	CQ	1570	X-RAY DIFFRACTION	POSITIONAL	0.042
4	58	CR	1570	X-RAY DIFFRACTION	POSITIONAL	0.043
4	59	CS	1570	X-RAY DIFFRACTION	POSITIONAL	0.039
4	60	CT	1570	X-RAY DIFFRACTION	POSITIONAL	0.04

LS refinement shell

Resolution (Å)	Rfactor Rfree	Num. reflection Rfree	Rfactor Rwork	Num. reflection Rwork	Refine-ID	% reflection obs (%)
3.7-3.742	0.3274	974	0.3202	18519	X-RAY DIFFRACTION	85
3.742-3.786	0.3226	989	0.3171	19551	X-RAY DIFFRACTION	89
3.786-3.8322	0.3148	1107	0.2977	21037	X-RAY DIFFRACTION	97
3.8322-3.8807	0.3153	1101	0.2946	21747	X-RAY DIFFRACTION	100
3.8807-3.9317	0.3005	1183	0.2865	21685	X-RAY DIFFRACTION	100
3.9317-3.9856	0.3076	1149	0.2803	21751	X-RAY DIFFRACTION	100
3.9856-4.0425	0.2901	1153	0.2735	21737	X-RAY DIFFRACTION	100
4.0425-4.1028	0.2806	1207	0.2664	21761	X-RAY DIFFRACTION	100
4.1028-4.1669	0.2626	1149	0.2583	21682	X-RAY DIFFRACTION	100
4.1669-4.2352	0.2712	1129	0.2504	21813	X-RAY DIFFRACTION	100
4.2352-4.3081	0.2512	1135	0.2409	21702	X-RAY DIFFRACTION	100
4.3081-4.3864	0.2426	1071	0.2349	21846	X-RAY DIFFRACTION	100
4.3864-4.4708	0.2534	1146	0.2292	21835	X-RAY DIFFRACTION	100
4.4708-4.5619	0.2261	1154	0.2268	21724	X-RAY DIFFRACTION	100
4.5619-4.6611	0.2441	1196	0.2193	21733	X-RAY DIFFRACTION	100
4.6611-4.7694	0.2286	1151	0.2164	21785	X-RAY DIFFRACTION	100
4.7694-4.8886	0.2318	1164	0.214	21774	X-RAY DIFFRACTION	100
4.8886-5.0206	0.2287	1123	0.2164	21802	X-RAY DIFFRACTION	100
5.0206-5.1682	0.2323	1109	0.2143	21860	X-RAY DIFFRACTION	100
5.1682-5.3349	0.2492	1152	0.2227	21787	X-RAY DIFFRACTION	100
5.3349-5.5253	0.2545	1165	0.2329	21763	X-RAY DIFFRACTION	100
5.5253-5.7462	0.2389	1127	0.2291	21825	X-RAY DIFFRACTION	100
5.7462-6.0073	0.2492	1183	0.224	21825	X-RAY DIFFRACTION	100
6.0073-6.3235	0.2382	1152	0.2226	21839	X-RAY DIFFRACTION	100
6.3235-6.7188	0.2425	1166	0.218	21820	X-RAY DIFFRACTION	100
6.7188-7.2361	0.2125	1182	0.1964	21846	X-RAY DIFFRACTION	100
7.2361-7.9616	0.202	1171	0.183	21851	X-RAY DIFFRACTION	100
7.9616-9.1076	0.1822	1224	0.166	21870	X-RAY DIFFRACTION	100
9.1076-11.4516	0.1619	1082	0.1547	22028	X-RAY DIFFRACTION	100
11.4516-49.804	0.267	1201	0.2584	22107	X-RAY DIFFRACTION	100

Refinement TLS params.

Method: refined / Refine-ID: X-RAY DIFFRACTION

ID	L11 (°2)	L12 (°2)	L13 (°2)	L22 (°2)	L23 (°2)	L33 (°2)	S11 (Å °)	S12 (Å °)	S13 (Å °)	S21 (Å °)	S22 (Å °)	S23 (Å °)	S31 (Å °)	S32 (Å °)	S33 (Å °)	T11 (Å2)	T12 (Å2)	T13 (Å2)	T22 (Å2)	T23 (Å2)	T33 (Å2)	Origin x (Å)	Origin y (Å)	Origin z (Å)
1	0.0616	0.07	-0.171	0.3466	0.3089	0.5787	0.1108	0.484	0.2704	0.1185	-0.2579	-0.1895	-0.2085	-0.1079	-0.7186	0.6273	0.1804	-0.0113	0.9348	0.5743	0.477	13.5248	103.453	53.6394
2	0.2838	0.1222	0.0809	0.1679	-0.1676	0.1134	0.104	-0.0694	0.4267	-0.0168	-0.1493	0.1453	-0.1113	0.0626	-0.0035	0.5176	0.1515	0.0035	0.7372	0.5342	0.6362	12.6932	111.9041	79.4654
3	0.069	-0.0228	-0.0718	0.0314	0.0171	0.0539	-0.0702	-0.1636	-0.0771	-0.0032	0.0097	0.2795	0.0297	0.1804	-0	0.5994	0.2625	-0.0982	0.8561	0.4601	0.6425	-21.5722	99.7776	63.3746
4	0.0809	-0.1747	-0.1371	0.6568	0.2734	0.317	-0.1594	0.1313	-0.0206	-0.2841	-0.2454	0.4318	0.011	-0.198	-0.1205	0.5904	0.2593	-0.1104	0.764	0.6203	0.3423	-19.9936	92.0382	61.6009
5	0.0245	0.135	-0.161	0.8609	0.2122	0.4082	-0.2499	0.2282	0.2334	-0.028	-0.0946	0.4859	0.0673	0.0755	-0.2529	0.5801	0.0917	-0.1985	1.1763	0.3632	0.1887	-20.4558	54.4658	28.918
6	0.1701	0.0332	0.0607	-0.0115	0.0895	0.2245	-0.1279	0.2356	0.3236	-0.1629	0.1056	0.0008	-0.075	-0.0861	0.1065	0.8026	0.1623	-0.0241	1.0996	0.5878	0.0838	-5.1193	76.8342	31.0763
7	0.0038	-0.0083	0.0233	0.0292	-0.0422	0.0415	0.1737	0.5702	0.0563	0.3499	-0.0898	0.0843	-0.0756	0.2037	-0.0012	0.525	0.1863	-0.2311	0.8823	0.4185	0.5565	-38.554	75.7074	52.5771
8	0.1454	-0.1785	0.0659	0.5088	0.3018	0.2701	-0.2097	0.2607	0.0396	0.2631	-0.1377	0.3503	0.3777	0.1047	-0.0372	0.6535	0.1647	-0.1441	0.8899	0.292	0.4032	-37.2774	69.3268	57.3979
9	0.1472	-0.2355	-0.1579	0.3052	0.2332	0.1363	-0.0366	0.3909	0.0803	0.1886	0.0501	0.1468	0.0664	0.0218	-0.0766	0.3858	0.1328	-0.0626	0.6784	0.1162	0.1009	-53.01	26.3238	76.9587
10	0.0683	-0.128	-0.0467	0.2582	0.106	0.018	-0.0226	0.0568	-0.0124	-0.1982	-0.0535	0.3354	-0.2618	-0.3301	-0	0.6087	0.2217	-0.0724	0.8936	0.2161	0.2733	-44.5503	33.3149	52.0589
11	0.0548	0.0562	-0.0131	0.0613	-0.0172	-0.0092	0.0417	0.0752	-0.0265	0.196	-0.1454	0.0949	0.1557	-0.0346	0	0.3984	0.2524	-0.037	0.9747	0.2926	0.4281	-53.8072	62.9764	76.7904
12	0.1128	-0.2685	0.0312	0.5243	-0.071	-0.0183	0.0737	0.3559	0.2435	0.1789	-0.324	0.1455	-0.0762	-0.0345	-0.0561	0.3755	0.1556	-0.124	0.7506	0.3021	0.38	-48.5074	61.8882	82.8176
13	0.3293	-0.0126	0.3408	0.1501	0.005	0.1809	-0.1535	0.1936	0.3042	0.1126	-0.165	0.2435	0.0408	-0.023	-0.0075	0.4619	0.1283	0.0457	0.4063	0.0464	0.3569	-38.9271	57.7	131.5486
14	0.0266	-0.2275	-0.011	0.7265	-0.065	-0.0175	0.2607	0.0947	0.2521	0.0306	-0.1902	0.6436	0.0295	0.13	-0.0066	0.4184	0.1552	0.0338	0.4164	0.096	0.2601	-50.8433	41.0761	113.6236
15	0.0539	0.0331	0.0535	0.0153	0.0316	0.0261	-0.0097	-0.2655	0.1964	0.1285	-0.0338	0.275	0.0361	0.102	-0	0.5955	0.2212	-0.0111	0.778	0.1816	0.7565	-46.2317	78.9984	102.6266
16	0.1313	0.1687	0.1616	0.1637	0.1767	0.1596	-0.0851	0.1936	0.228	0.145	-0.2321	0.0862	-0.396	0.0994	-0.0087	0.4295	0.1967	-0.102	0.6207	0.2285	0.5004	-38.1775	79.8506	102.7659
17	0.1803	0.1481	-0.1796	0.4362	-0.1657	0.1596	0.2176	0.2585	0.3488	0.0864	-0.0513	0.0374	-0.1031	-0.0214	-0	0.4104	0.1487	0.0546	0.4119	0.3047	0.6266	2.1089	105.4794	117.1501
18	0.2719	-0.1445	0.2585	0.1609	0.0275	0.1561	0.1165	-0.0321	0.2031	0.1634	0.0943	0.2004	-0.2627	-0.0573	0	0.5145	0.0946	-0.009	0.4527	0.1593	0.573	-15.4502	89.605	130.5696
19	0.1428	0.0626	-0.0324	0.0248	-0.0298	0.0193	0.1333	0.1561	-0.1276	-0.0281	-0.1904	-0.1261	-0.1911	0.2649	0	0.4925	0.246	-0.0343	0.6475	0.437	0.7385	-26.3352	101.7966	94.323
20	0.1253	-0.1684	0.0032	0.2074	0.2082	0.1707	0.0384	0.0215	-0.0116	0.0074	0.0681	0.1749	-0.2234	-0.0803	-0	0.4986	0.1549	-0.0279	0.6921	0.4408	0.7424	-20.5915	98.5803	89.6364
21	0.1203	0.0899	0.0944	0.0796	0.0284	-0.0252	0.2719	-0.1415	-0.219	0.2434	-0.1166	-0.2681	0.0619	0.0312	0.0063	0.3849	0.1019	-0.3931	0.1936	0.0569	1.0722	96.0508	-103.8826	161.9727
22	0.2449	-0.0827	0.2225	0.0483	-0.0425	0.1601	0.0074	-0.0453	-0.2177	0.0252	0.0004	-0.4769	0.1842	-0.1868	0	0.4383	0.1275	-0.2054	0.2669	0.0011	0.9291	72.0021	-113.1937	153.3543
23	0.0735	0.0472	-0.0698	0.0089	-0.0404	0.0504	-0.0275	0.1895	0.026	-0.1158	0.1115	0.0779	0.1957	0.2883	0	0.7978	-0.0006	-0.3787	0.324	0.3256	1.0461	74.371	-102.2382	191.5024
24	0.1117	-0.1658	-0.0158	0.1227	-0.0236	0.0294	0.0592	0.0124	-0.4144	0.316	-0.0557	-0.1531	0.0834	-0.0827	-0.0004	0.5509	0.006	-0.3098	0.2207	0.2402	0.8347	76.2215	-94.3771	190.908
25	0.2441	-0.1682	0.0288	0.1349	-0.2646	0.369	0.3819	-0.1844	-0.2847	0.5238	-0.1209	-0.0115	0.0743	0.0056	0	0.786	-0.1318	-0.3575	0.3461	0.2086	0.8048	104.7791	-55.7533	204.0818
26	0.114	0.0934	0.0528	0.1741	0.014	0.4298	-0.0729	0.0574	-0.3753	-0.0863	-0.0566	-0.288	0.1948	0.0547	-0.0003	0.6105	0.0939	-0.4822	0.2903	0.166	1.0344	109.2071	-77.4091	188.2438
27	0.0564	-0.0878	0.0159	0.0936	-0.0097	-0.006	0.0008	-0.1035	-0.0612	-0.25	0.1795	-0.047	-0.1795	0.2295	0	0.9262	-0.0396	-0.1575	0.4815	0.3055	0.7134	77.3499	-78.7859	212.0015
28	0.1471	0.0324	-0.0097	0.1753	0.1516	0.1434	0.1499	-0.0827	-0.0667	0.1479	-0.0903	0.0121	0.0844	0.1577	0	0.8065	-0.0387	-0.3261	0.2833	0.3129	0.6264	72.9701	-72.5109	209.3498
29	0.3836	0.2069	0.0412	0.1094	-0.0725	0.1495	-0.1053	-0.2032	-0.0308	0.0007	-0.0162	-0.2709	0.055	0.0028	0	0.7211	-0.0547	-0.1931	0.2769	0.1464	0.3557	47.2698	-30.9905	218.858
30	0.1002	-0.0999	-0.1507	0.3005	-0.0708	0.0922	0.1022	-0.2127	0.096	0.1722	-0.137	-0.2749	0.1618	0.0362	-0	0.731	-0.1894	-0.3371	0.4403	0.1993	0.5227	73.8305	-36.7326	219.3811
31	0.0484	0.0084	0.0456	0.0093	-0.0221	0.0542	0.3926	0.1222	0.1812	0.1217	-0.1192	0.2732	-0.1444	0.2042	-0	0.8803	-0.1507	-0.232	0.5583	0.3718	0.3934	48.8641	-67.6829	218.213
32	-0.0446	-0.021	0.0515	0.167	-0.1279	-0.0152	0.1064	-0.3006	-0.2418	0.0272	-0.2629	0.0966	-0.0999	-0.0333	-0	0.9151	-0.1355	-0.2114	0.3439	0.2216	0.4618	45.0189	-66.5026	211.1867
33	0.1938	0.0208	0.0362	0.0689	0.1278	0.2041	0.1218	-0.1164	0.0942	0.2138	-0.0778	-0.0749	-0.0857	-0.0319	-0.2485	0.6934	-0.0787	0.0827	0.1883	0.1549	0.1439	2.8328	-63.2413	185.0246
34	0.2395	0.3068	0.2462	0.3512	0.2509	0.0611	-0.0889	-0.1037	-0.1882	0.0587	-0.0344	-0.2175	-0.0503	-0.1913	-0.0001	0.7479	-0.0771	0.0033	0.284	0.0926	0.1808	14.5134	-46.7737	203.2457
35	0.0269	-0.0034	0.0546	0.031	0.0111	0.0916	-0.3137	-0.0259	-0.162	0.1261	-0.0931	-0.195	-0.4056	-0.0038	0	0.8426	-0.1527	0.0187	0.258	0.2206	0.4832	28.3649	-84.0106	201.2828
36	0.7329	-0.4992	0.2018	0.3479	-0.2008	0.1179	-0.0812	0.3475	-0.1199	0.2355	-0.169	-0.1403	-0.014	0.1676	-0.3239	0.6252	-0.1296	-0.1071	0.1057	0.2071	0.3578	31.1238	-84.4012	193.6822
37	-0.0189	0.0263	-0.0064	0.2003	-0.0654	-0.0093	0.0679	0.056	-0.312	0.349	0.0113	0.0948	0.2054	0.209	0.0005	0.4122	0.0687	-0.0636	0.1721	0.0218	0.592	32.8477	-108.5852	150.1058
38	1.1825	-0.6156	0.3549	0.2884	-0.1854	0.0658	-0.127	0.2403	-0.3688	0.2057	0.0574	0.0302	-0.127	0.0744	-0.0618	0.6115	-0.0561	0.0671	0.1576	0.1559	0.4121	13.415	-93.9385	162.2437
39	0.023	0.0165	-0.0294	0.0121	-0.0028	0.0296	0.3335	0.0394	-0.3418	-0.1727	-0.3245	0.0201	-0.1481	0.2971	0	0.6588	0.0238	-0.0682	0.1766	0.2708	0.8232	44.0402	-105.4462	184.9074
40	0.0113	0.0779	0.0331	0.1937	0.1297	0.0693	0.0392	-0.068	-0.2777	0.0158	-0.0056	-0.0807	0.1652	-0.0131	-0	0.7358	-0.0436	-0.1061	0.2609	0.1869	0.6093	50.3036	-101.8276	181.2822
41	0.9799	-0.1105	-0.243	-0.0074	-0.0091	0.0283	0.2165	0.0417	0.394	0.1353	-0.1169	-0.021	0.0543	-0.0702	0.3128	0.7295	-0.1088	-0.1649	0.3326	-0.2503	0.2196	54.9153	20.8203	222.1199
42	0.1622	-0.07	-0.1478	0.1945	0.007	0.099	0.1478	-0.181	-0.0772	0.424	-0.1563	0.0951	-0.0338	-0.0078	-0	0.8836	-0.0866	-0.035	0.3455	-0.0395	0.2419	36.7247	0.6338	221.4633
43	0.0664	0.0643	-0.0847	0.0744	-0.0926	0.086	0.1012	0.1524	0.1272	0.1334	0.1884	0.0485	-0.0118	-0.003	-0	0.9972	-0.0469	0.1035	0.4415	-0.2074	0.3939	22.3816	37.6396	224.4371
44	0.7078	-0.5316	-0.0736	0.4964	0.0824	0.2243	0.0619	0.1751	0.2134	0.3804	-0.2499	-0.0901	0.05	-0.0618	-0.4505	0.6961	-0.0607	0.0313	0.2937	-0.2047	0.0565	25.0309	41.0558	217.5905
45	0.0041	0.048	0.1564	0.0021	0.1108	0.3056	-0.0609	0.0643	0.3853	0.2415	-0.0183	-0.047	0.0171	-0.0602	-0.0004	0.5244	-0.0278	0.0261	0.3021	-0.1135	0.4515	47.8404	78.7839	194.2523
46	0.067	0.0279	-0.0225	0.0542	-0.0336	0.0058	0.1036	0.118	0.1074	0.3875	-0.1117	-0.1426	0.0946	-0.0399	-0.0011	0.5496	-0.0878	-0.0079	0.2146	-0.153	0.3375	57.0786	58.6427	210.0715
47	0.0276	-0.0047	-0.0171	0.0074	0.0045	0.0733	-0.2281	-0.0432	0.1578	0.1059	0.1663	0.0952	0.0572	0.147	0	0.7503	0.0116	0.0753	0.4396	-0.1585	0.3668	17.8528	65.1769	210.4228
48	0.2448	0.0842	-0.2988	0.2732	-0.2153	0.3644	-0.0221	-0.1417	0.2085	0.1597	0.1111	0.1219	-0.0555	0.1153	0.098	0.5911	-0.0676	0.1246	0.2756	-0.1884	0.1804	15.8254	63.8213	202.6988
49	0.3309	0.2214	0.1808	0.0974	0.0496	0.1284	-0.0578	-0.0119	0.2776	0.02	-0.0265	-0.0774	0.1958	-0.1955	-0.0016	0.466	0.0066	0.0858	0.3785	0.0296	0.2723	-7.6118	78.4803	161.3192
50	0.1482	-0.1065	-0.1566	0.091	0.1646	0.2017	-0	-0.0517	0.3073	0.0172	-0.0421	0.354	0.0122	0.06	-0	0.486	-0.0284	0.1394	0.26	-0.0258	0.4776	15.1592	86.9705	173.5694
51	0.0011	0.031	-0.0581	0.3564	-0.1194	0.2417	0.0547	0.2688	0.1321	0.0294	0.381	0.233	-0.1834	-0.2328	0.011	0.6706	0.0005	0.0523	0.5127	-0.0592	0.2577	-9.0701	63.6891	194.7905
52	0.0263	0.0205	-0.182	-0.0097	-0.0569	0.1933	0.0188	-0.0985	0.1134	-0.0499	-0.0182	0.1406	0.2713	-0.1063	-0	0.6167	-0.0657	0.1482	0.2739	-0.1042	0.221	-9.13	56.8678	190.4217
53	0.6162	0.3013	-0.0448	0.1581	-0.0691	0.1273	0.2589	0.2299	0.2221	0.2228	-0.0607	0.0729	0.3215	0.1504	0.1729	0.749	-0.0487	0.213	0.3321	-0.1134	0.0964	-34.728	20.3688	168.4659
54	0.1188	0.4016	-0.0299	0.9758	-0.1919	0.1995	-0.1971	0.0985	0.0466	0.0122	-0.0017	0.5377	-0.155	0.0355	-0.0253	0.5244	0.0361	0.1382	0.292	-0.075	-0.097	-30.9666	46.5958	162.2574
55	0.0555	-0.1191	-0.0202	0.2111	0.0408	0.0785	-0.1515	-0.1634	0.0662	0.0074	0.0633	-0.3429	0.0263	-0.1794	-0.0127	0.7386	-0.0826	0.3192	0.285	-0.1492	0.2517	-21.2513	35.2048	198.9996
56	0.2449	0.2031	0.4386	0.1835	0.6806	1.4425	0.3088	-0.0782	-0.2936	0.1521	0.2276	-0.1159	0.0225	-0.1835	1.0926	0.7069	0.0287	0.2723	0.0857	-0.3863	-0.2904	-15.4052	29.7832	197.6366
57	0.0123	-0.0063	0.0276	0.7236	0.0583	0.4825	-0.0031	-0.1949	-0.0578	-0.036	0.2083	-0.8096	0.1683	-0.093	0.4593	0.7636	0.0152	0.0183	0.3125	0.0104	-0.2806	3.8704	-15.2396	205.9418
58	0.3169	-0.2235	-0.0493	0.4132	0.2152	0.1962	0.2807	-0.399	-0.2373	-0.0885	-0.1839	0.5326	-0.1585	-0.1619	0.457	0.7427	0.0043	0.146	0.3175	-0.1635	-0.282	-17.6299	-6.6813	191.6537
59	0.065	0.0369	-0.0111	-0.0072	0.0076	-0.004	-0.0618	-0.3034	0.0473	0.1632	-0.3311	0.2972	0.1778	0.2282	-0	0.7743	-0.0775	0.0978	0.4798	-0.1537	0.3038	-1.8427	19.0807	217.3673
60	-0.0022	-0.0072	0.041	0.1022	0.1666	0.1013	0.1539	-0.2914	-0.0523	-0.0501	-0.0524	-0.1844	-0.06	-0.0805	0.279	0.7835	-0.0575	0.1881	0.4156	-0.1835	-0.0892	5.6701	19.9967	214.5087
61	0.1353	-0.0188	0.1537	-0.0484	-0.0711	0.0635	-0.124	0.0404	-0.2394	-0.1062	-0.072	0.0476	0.0161	-0.0327	-0.038	0.3552	0.0458	-0.0094	0.6236	-0.3384	0.2891	-24.7977	-82.5934	81.2075
62	0.1496	-0.1704	0.0476	0.2473	-0.2832	0.2498	0.1838	0.3045	-0.1986	-0.3092	-0.0945	0.1509	-0.2	-0.0329	0.4966	0.3777	-0.0268	-0.0286	0.6927	-0.2909	0.1738	-37.3491	-62.5837	67.7298
63	0.0517	0.0109	0.0001	0.1602	-0.0804	0.0186	0.1559	0.1477	-0.3049	-0.4334	0.1525	-0.3835	0.1917	-0.2145	-0.0016	0.3666	0.0902	-0.1458	0.6805	-0.2183	0.4458	-51.1078	-71.1954	104.0246
64	0.3184	0.1295	-0.1106	-0.0313	-0.029	0.0264	-0.0486	0.2469	-0.2148	0.158	-0.0335	0.2058	0.343	-0.1721	0	0.3748	0.0343	-0.0164	0.5162	-0.2121	0.4257	-44.6717	-69.6796	108.7
65	-0.0391	0.0171	0.0846	-0.0403	0.0432	0.2854	-0.1322	0.0901	-0.1959	0.0777	0.0318	-0.0874	0.1304	-0.0804	0.0099	0.4317	-0.0611	0.0762	0.1989	-0.022	0.1866	-13.1765	-83.7882	144.6021
66	0.1847	-0.0057	0.1343	0.0665	-0.0769	0.1496	0.1154	0.274	-0.4129	0.228	-0.0933	0.0875	-0.02	0.0801	-0	0.3679	-0.0486	0.0178	0.3922	-0.1979	0.4139	-16.4569	-91.6453	118.7752
67	0.0943	0.0367	0.0618	0.0604	-0.0499	0.069	-0.1119	0.3675	0.0898	0.5072	0.1485	0.2048	-0.0864	0.0526	0	0.4863	-0.0652	0.1358	0.4802	-0.1455	0.392	-45.9594	-70.4978	134.9435
68	0.4305	0.1307	0.1932	0.2642	-0.0315	0.0122	-0.1576	0.179	-0.2109	0.2355	-0.0683	0.0598	0.046	-0.1323	-0.0408	0.3934	-0.0438	0.0673	0.313	-0.0428	0.112	-42.2813	-63.4985	136.6882
69	0.3106	0.2826	0.2869	0.2711	0.2197	0.1559	-0.1746	0.0338	0.2151	0.0298	-0.0163	0.421	-0.0713	0.1775	-0.2072	0.4152	0.0667	0.1354	0.1705	-0.0859	0.0497	-32.2223	-27.4148	169.5317
70	0.5938	-0.3818	-0.4091	0.3238	0.1534	0.3548	-0.1683	0.019	-0.3552	0.3687	-0.104	0.3027	0.1629	-0.1136	-0.2886	0.4945	-0.0561	0.1324	0.2476	0.0317	0.153	-23.756	-53.1514	167.3855
71	0.0209	0.0294	0.0015	0.0333	0.0282	0.0294	0.0561	0.1121	-0.233	0.4445	-0.103	-0.0035	-0.1536	0.0817	-0	0.4496	-0.1072	0.1651	0.4694	-0.1634	0.5665	-55.5221	-42.8228	145.8041
72	0.3028	0.1731	0.0619	0.0286	0.0247	0.0052	-0.1561	-0.0178	-0.0885	0.1184	-0.057	0.0543	0.0574	-0.1367	-0	0.3027	-0.0577	0.0466	0.2319	-0.1317	0.2327	-52.5215	-37.031	141.0011
73	0.0196	0.0293	-0.0749	0.2725	-0.1477	0.0959	-0.1437	0.027	-0.0854	0.0267	0.0728	-0.0523	-0.025	-0.1093	0	0.3355	0.0462	0.0244	0.4518	0.0122	0.1981	-55.4944	8.7472	121.5355
74	0.3359	0.298	0.0787	0.197	0.0295	-0.0155	0.0103	-0.0236	-0.1215	0.2059	-0.0321	0.2435	-0.1861	0.0387	-0.0002	0.376	-0.0246	0.0338	0.3418	-0.0314	0.1666	-49.2968	-0.3589	146.4154
75	0.0583	-0.0084	-0.0756	0.0332	0.0432	0.0622	-0.1233	-0.0562	-0.0743	0.237	-0.0615	-0.2901	0.076	-0.1634	0	0.1807	0.0271	-0.0393	0.5924	-0.1248	0.4521	-66.5831	-26.2071	121.6774
76	0.1879	0.0461	-0.0582	0.0365	-0.0515	0.1643	-0.0775	0.0003	-0.2897	0.0382	0.0166	0.2593	-0.0744	-0.0784	0.0003	0.2269	-0.0141	0.0096	0.502	-0.0711	0.1919	-61.1972	-26.6569	115.6491
77	0.247	-0.1152	0.1878	0.1291	0.0813	0.1277	-0.0877	0.1654	0.0103	0.0234	-0.226	0.0947	0.1476	-0.2059	-0.0109	0.4054	-0.0064	-0.044	0.7845	-0.222	0.1638	-50.982	-25.3195	66.8852
78	0.1079	-0.0324	-0.1739	0.1975	-0.0674	0.1913	0.0754	0.2156	0.0158	-0.0744	-0.13	0.2873	-0.1232	0.1393	0	0.3905	0.0211	-0.0455	0.6971	-0.0889	0.2935	-57.6577	-6.0459	84.8609
79	0.0792	-0.0303	-0.0888	-0.0029	0.0232	0.0546	0.261	-0.2172	-0.2398	-0.0428	-0.0751	0.2769	0.1889	0.1976	0.0013	0.2636	-0.001	-0.0231	0.6826	-0.3266	0.5332	-63.8838	-43.7589	95.8675
80	0.6444	-0.3101	-0.31	0.2237	0.1373	0.1904	0.0155	-0.0828	-0.3401	-0.2269	-0.0418	0.2647	0.2057	0.1204	0.0208	0.2331	-0.093	-0.0487	0.6019	-0.3472	0.1688	-56.3998	-46.8481	95.6956
81	0.8689	-0.6168	0.0442	0.5632	-0.2027	0.124	-0.1743	0.1703	-0.6336	-0.3337	0.2627	0.4049	-0.2767	-0.0655	-0.2284	0.6175	0.0405	-0.2399	1.1171	-0.039	-0.1696	-36.5265	9.2288	29.8665
82	0.3546	-0.0252	-0.231	0.1518	-0.1625	0.2361	-0.0455	0.2491	0.2148	-0.0478	0.295	0.0749	0.3984	-0.1259	0.5867	0.4893	-0.0044	-0.2109	1.0298	-0.0971	0.0576	-40.3518	-16.974	36.0999
83	0.0304	0.0598	0.0365	0.0471	0.024	0.0096	-0.0689	0.0611	0.1647	0.2721	0.2768	-0.2867	0.0337	-0.361	-0	1.023	0.0051	-0.1311	1.6444	-0.057	0.4164	-27.8006	-8.8321	-0.6953
84	-0.0079	0.0626	0.0845	0.0956	0.2283	0.3669	-0.0194	0.2858	0.1214	-0.1231	0.3508	-0.1437	0.0446	0.0151	0.6365	0.9012	-0.1065	-0.1877	1.3282	-0.2458	-0.3855	-20.6554	-5.289	0.6862
85	1.2543	0.0574	0.01	0.0472	-0.0459	-0.0045	-0.0631	0.6625	-0.2869	0.0839	0.245	-0.0808	-0.2612	-0.0638	0.0739	1.0017	0.0258	0.0111	1.4328	0.1645	-0.1453	10.839	32.4623	-7.468
86	0.2482	0.2924	0.2976	0.2117	0.2366	0.2593	0.1777	0.3353	0.3655	-0.0504	-0.0293	0.158	-0.1846	-0.143	0.0077	0.8457	-0.0189	-0.1046	1.2992	0.2197	0.0454	-12.2821	30.383	6.697
87	0.0411	0.0249	-0.0084	0.0045	0.0116	0.0149	-0.3203	0.0736	-0.2968	-0.1668	0.0184	0.065	-0.0196	-0.0626	-0	0.9781	-0.0464	0.0131	1.5921	-0.0862	0.1508	-4.2438	1.2379	-18.9725
88	0.2247	-0.19	0.3026	0.2815	-0.1978	0.2138	-0.236	0.4083	0.1346	-0.1599	0.2797	-0.2737	0.1668	-0.1559	0.0015	0.9393	-0.1433	0.0946	1.5127	-0.1012	-0.109	2.652	-1.7877	-16.0572
89	1.0902	-0.4409	-0.1072	0.2825	-0.1412	0.172	0.3816	-0.2393	-0.3863	-0.521	-0.0327	-0.1182	-0.025	0.0242	0.1732	1.0789	-0.1367	0.162	1.5275	-0.4252	-0.0103	49.7712	-16.4357	-23.4217
90	1.4095	-0.7265	-0.088	0.429	0.1596	0.1627	-0.2685	0.1733	0.7215	-0.3678	0.3043	-0.3201	0.1053	0.0719	0.0043	1.185	-0.1221	0.0992	1.4956	-0.0366	-0.0525	37.9406	8.0431	-22.8498
91	0.1151	0.129	-0.0113	0.1182	0.0158	0.0635	0.1165	-0.1003	0.0993	-0.2831	0.1263	0.0833	0.1721	0.1153	0.0007	1.2833	-0.0904	-0.129	1.7608	-0.357	0.0678	13.9357	-23.4533	-25.9842
92	0.4684	0.2083	0.0975	0.197	0.0032	0.0268	-0.3002	0.045	-0.3809	-0.2325	0.1121	-0.1449	0.3528	-0.0229	-0.0834	0.9892	-0.191	0.0009	1.7503	-0.3753	-0.1301	15.4782	-27.482	-19.1347
93	0.514	-0.0386	0.2523	0.0272	-0.0674	0.3616	-0.2512	-0.029	-0.4982	-0.2303	0.3647	-0.2431	-0.0447	-0.1525	-0.0077	0.7722	-0.109	0.0557	1.2442	-0.5439	0.341	26.7085	-69.8907	4.3751
94	0.174	0.1372	0.0836	0.0786	0.0324	0.1059	0.0294	0.4947	-0.1497	-0.2636	0.0115	-0.3643	-0.2795	-0.0914	-0	0.8485	-0.1106	0.1319	1.4125	-0.4363	0.3721	41.1832	-53.2242	-11.4983
95	0.1266	0.1262	-0.0254	0.1131	-0.024	0.1085	0.1019	-0.2158	-0.2706	-0.0146	-0.0695	-0.183	-0.2919	0.1949	0.0008	0.8395	-0.1043	-0.0285	1.5884	-0.375	0.0995	1.6617	-48.5521	-11.8946
96	0.0833	-0.0514	-0.0403	-0.0819	-0.0149	0.0621	-0.2031	0.1068	-0.0991	-0.1583	0.1033	-0.0987	-0.1322	-0.0855	-0.1523	0.7963	-0.1488	-0.0306	1.3399	-0.6838	-0.2988	0.1097	-46.6289	-4.2
97	0.7584	0.0638	-0.0902	0.2699	0.0454	-0.0409	-0.151	0.1854	-0.971	0.2395	-0.0553	-0.298	-0.0661	-0.011	-0.7009	0.4605	-0.019	-0.2269	0.9878	-0.5786	-0.4295	-26.684	-54.1212	37.0506
98	1.303	0.3508	-0.2872	0.1881	-0.066	0.3024	-0.0367	0.0414	-0.7336	-0.1804	-0.2065	-0.1183	0.1457	0.2598	-0.3778	0.6202	0.0098	-0.0764	1.0162	-0.5931	0.034	-7.0026	-68.4785	24.9238
99	-0.0009	-0.0009	-0.0015	-0.0005	0.0197	0.0574	0.0741	-0.1586	-0.3048	0.2242	0.3214	-0.28	0.2531	0.1618	-0	0.8666	-0.0089	-0.0532	1.456	-0.2843	0.3026	-24.0102	-39.6274	3.5128
100	0.0451	0.0122	-0.0039	0.3234	-0.5402	0.9095	0.3533	0.002	-0.0039	-0.0918	0.2676	0.4357	-0.0572	0.0308	0.7391	0.8722	0.0055	-0.1701	1.3557	-0.4994	-0.2884	-22.2464	-33.0172	7.8456
101	0.1017	0.1287	0.0053	0.0925	0.1789	0.2311	-0.149	0.059	-0.3729	0.1835	0.0837	-0.2911	0.0904	0.2552	0	0.3426	0.1113	-0.5126	0.4626	0.0086	1.7354	177.1054	-31.6443	149.7278
102	0.0984	0.0313	-0.0787	0.0424	-0.0614	0.0807	0.0477	0.0196	-0.1157	-0.0118	-0.2084	-0.522	-0.0825	0.0744	0	0.2843	0.1129	-0.2544	0.4472	-0.1247	1.8021	187.1166	-28.357	124.6936
103	0.0495	0.0073	-0.0083	-0.0065	-0.0059	0.003	-0.0572	0.19	0.1227	-0.1812	0.1763	-0.2132	-0.3033	-0.3257	-0	0.3393	0.1608	-0.4228	0.6486	-0.0418	2.1212	182.5427	-65.7959	137.4246
104	0.0284	-0.0556	-0.0549	0.0344	0.0225	0.0064	0.2263	0.3027	-0.0034	0.0328	-0.0542	-0.3906	0.0225	-0.1266	-0	0.3216	0.1648	-0.3496	0.517	-0.1526	1.9891	174.5534	-66.2111	138.6844
105	0.1627	0.2579	0.0248	0.2298	0.087	0.0641	0.0891	0.0759	-0.43	0.0458	-0.1888	-0.5065	-0.3085	-0.004	0.0002	0.4188	0.1301	-0.5681	0.2877	0.1425	1.474	136.034	-77.9939	168.0118
106	0.0685	-0.0961	0.0089	0.2225	-0.0013	-0.0018	0.0324	-0.0122	0.1158	0.3375	0.0787	-0.567	0.1983	0.1165	0	0.3686	0.0791	-0.5292	0.3672	0.081	1.4603	154.2524	-57.7971	168.71
107	0.0228	-0.0221	0.0179	0.0202	-0.0077	-0.0022	-0.2114	-0.3262	0.1985	-0.0924	-0.065	0.0401	0.2232	0.1019	0	0.5026	0.1486	-0.4702	0.4263	0.0303	1.9877	162.601	-88.6736	145.1447
108	0.3401	-0.2888	-0.2694	0.212	0.2427	0.2426	-0.0906	0.3106	-0.1284	0.3458	0.0584	-0.2595	0.2591	-0.2404	-0.0904	0.1381	0.1656	-0.4561	0.2386	-0.0566	1.9576	156.4512	-88.5049	139.8812
109	0.1389	0.0234	0.2083	0.1295	-0.0482	0.159	0.0044	0.2094	-0.0734	0.2315	-0.0254	-0.3778	0.0773	-0.031	0	0.3056	0.1555	-0.2172	0.2283	-0.174	1.414	119.7793	-112.1372	115.7479
110	0.1999	-0.2023	-0.2316	0.289	0.0611	0.2238	-0.2578	-0.2803	-0.1492	-0.0141	0.0708	-0.2738	0.2456	0.1203	0	0.4269	0.1654	-0.3337	0.378	-0.0848	1.4306	122.8051	-104.3667	141.6352
111	0.0153	0.0074	0.0071	0.0187	-0.0159	0.0176	-0.1207	-0.1063	0.0734	-0.1359	-0.1632	0.1699	0.4923	-0.2306	-0	0.5311	0.2409	-0.3537	0.6028	-0.1974	1.8157	155.4497	-104.4357	118.971
112	0.1053	-0.0266	0.0678	0.0399	-0.0821	0.0564	-0.1479	0.0542	-0.056	-0.2037	0.0763	-0.3896	0.0444	0.0387	-0.0027	0.2035	0.146	-0.2486	0.46	-0.2446	1.8479	153.5606	-99.0304	113.2445
113	-0.0065	-0.0037	-0.1025	-0.0276	0.0426	0.3119	-0.053	0.3058	-0.4241	-0.0309	-0.3266	-0.1266	-0.0061	-0.0145	-0	0.4202	0.2385	0.1213	0.7982	-0.4873	1.7992	150.6072	-86.6622	65.0477
114	0.2857	-0.145	-0.0102	0.0135	-0.0147	-0.0107	-0.0631	0.1157	-0.0281	-0.1881	0.1776	-0.6381	0.012	-0.0471	0	0.3037	0.1133	0.0008	0.7073	-0.4248	1.3804	136.1059	-103.5579	80.7064
115	0.0158	0.0342	-0.0271	0.0454	-0.0376	0.0048	-0.1035	-0.105	0.149	-0.2094	0.0996	-0.1787	0.0571	0.0631	0	0.3172	0.2182	-0.0636	0.6543	-0.4384	2.081	170.9489	-91.1942	95.1423
116	0.0431	-0.0812	-0.0271	0.1153	0.0733	-0.0067	-0.1146	0.4538	-0.5725	0.0443	0.0637	-0.1494	-0.231	0.1486	0	0.3876	0.1209	-0.0672	0.5896	-0.2835	1.9238	169.8956	-83.1897	95.598
117	0.0701	0.1685	0.0679	0.0397	0.1772	0.034	-0.1578	0.2533	-0.4722	0.2669	0.1567	-0.5606	-0.111	-0.1006	0.0012	0.267	0.1493	0.0031	0.6726	-0.317	1.9151	186.0476	-36.9861	86.0002
118	0.2071	-0.1258	0.2302	0.0676	-0.0796	0.2058	0.2294	0.3291	-0.0767	-0.1067	0.2302	-0.1424	0.0322	0.0949	-0	0.2962	0.1262	0.1591	0.7611	-0.3528	1.8532	175.8671	-56.6103	70.203
119	0.0226	-0.0349	0.0078	0.0946	0.034	0.0035	-0.0378	0.2748	0.1281	0.2701	-0.1177	0.209	-0.5053	0.4337	0.0001	0.2445	0.0793	-0.1361	0.7529	-0.3582	2.0579	187.7904	-67.3144	106.6089
120	0.2299	-0.0092	-0.1509	0.1282	-0.1816	0.195	0.0318	0.2619	-0.2819	0.0692	0.0757	-0.1939	-0.0966	0.0854	-0	0.2356	0.1312	-0.1536	0.5509	-0.2073	2.0857	182.9535	-62.8851	111.3587
121	0.0212	0.061	-0.0733	0.2026	0.1016	0.1485	0.0792	0.046	-0.1488	-0.1069	-0.044	-0.195	0.1131	0.0712	0	0.4073	0.0295	-0.1195	0.3132	-0.1587	0.9986	68.5133	-122.8275	121.3873
122	0.0796	0.192	0.0964	0.2561	0.2455	0.172	-0.1432	0.1183	-0.3805	0.1762	0.0037	-0.0673	-0.007	0.0437	0	0.4572	0.104	-0.1299	0.4657	-0.3097	1.3746	90.0328	-123.4837	104.7491
123	0.0573	-0.0495	0.0069	0.0784	0.061	0.1273	0.1775	-0.2426	-0.0669	-0.3982	0.08	0.0516	0.2359	-0.1359	0.002	0.615	0.0743	0.1672	0.3766	-0.2499	1.0348	55.7034	-137.2985	90.2863
124	0.0611	0.1173	0.1381	0.0999	0.2267	0.118	-0.1201	0.0336	0.0377	-0.2494	-0.0242	-0.3963	0.019	-0.0227	-0	0.4228	0.0983	0.0077	0.2664	-0.3336	0.9037	50.9489	-130.7496	90.6277
125	0.1862	-0.042	0.2833	0.1005	-0.3012	0.516	0.0933	0.0041	-0.2965	-0.124	-0.2165	-0.0674	0.0535	0.0852	-0.0131	0.4414	0.0247	-0.0104	0.3894	-0.3106	0.6289	7.7355	-109.7383	103.8973
126	0.2545	0.2202	0.1873	0.1771	0.163	0.1303	0.1557	-0.1146	-0.2029	-0.0197	0.0395	-0.059	0.1312	-0.0171	-0	0.4725	0.0552	-0.0938	0.2624	-0.2114	0.7274	29.3079	-118.2056	118.1942
127	0.0585	-0.0445	-0.008	0.0631	-0.0356	0.0355	-0.2164	0.1766	0.1755	-0.0814	-0.0797	0.014	0.2186	-0.2596	-0	0.7638	-0.0237	0.0874	0.4885	-0.282	1.1412	26.5916	-130.6387	80.6256
128	0.0124	-0.1184	-0.0679	0.1723	0.1672	0.0628	0.1888	0.1539	-0.3313	0.041	-0.008	-0.4729	0.0836	-0.2636	-0.0007	0.4584	-0.016	0.102	0.4934	-0.5016	0.7977	26.8748	-123.6902	76.489
129	0.5733	0.297	-0.0581	0.5504	-0.1302	0	0.1991	-0.0769	-0.6338	-0.0562	-0.2984	-0.4631	0.1589	-0.2385	-0.6914	0.545	0.1318	0.1567	0.5352	-1.0369	-0.382	8.1477	-93.5384	41.5518
130	0.2289	-0.1346	0.3153	0.4922	-0.0781	0.3072	-0.0832	0.2616	-0.4435	0.1376	0.1501	0.1342	-0.1144	0.0295	0.0657	0.4616	0.1053	0.0472	0.6245	-0.503	0.5589	-0.4726	-100.6368	66.3541
131	-0.0168	0.0273	-0.0128	0.085	-0.0787	0.0615	-0.0211	0.1962	-0.0127	0.0286	0.2032	0.2329	-0.3506	-0.0451	-0	0.5907	-0.0793	0.1566	0.7649	-0.5608	0.8253	28.06	-123.0063	50.2369
132	-0.0109	-0.0226	-0.0125	0.2057	0.0447	0.1357	-0.2632	0.345	-0.3627	0.1783	-0.2048	-0.2491	0.082	0.0835	-0.0082	0.5455	-0.0574	0.0409	0.7779	-0.6314	0.7861	34.1017	-117.7057	49.3094
133	0.2343	0.079	0.156	0.196	-0.0144	0.0814	-0.0473	0.3224	-0.5599	-0.0575	0.0029	-0.359	-0.0336	-0.0285	-0.0055	0.6802	0.0421	0.1885	0.9731	-0.7398	0.911	68.9895	-96.9571	20.3577
134	0.053	-0.0763	-0.1223	0.191	-0.0444	0.1179	0.0569	0.3807	-0.1838	0.1626	-0.0172	-0.0915	-0.2758	-0.1189	0	0.6627	-0.1163	0.2271	0.991	-0.6825	0.6243	41.8916	-94.8946	21.0443
135	0.0481	0.008	0.0358	0.0291	0.0313	0.027	0.2676	-0.2726	0.1627	0.1294	0.0491	-0.1985	-0.4553	-0.0285	0	0.7068	0.0769	0.2592	0.7804	-0.5978	1.1482	58.069	-125.1044	41.2757
136	-0.0166	-0.0827	0.0198	0.2523	-0.1414	-0.0101	0.1625	0.2553	-0.3651	0.0074	-0.2876	-0.0298	0.0689	0.2093	0	0.6098	-0.0074	0.1306	0.7838	-0.6653	0.9573	62.6643	-121.2528	46.7166
137	0.0436	-0.139	-0.0503	0.1267	0.0814	0.0644	0.2542	0.03	0.1474	-0.2046	-0.1213	-0.3251	0.0816	-0.1426	-0	0.3512	0.0072	0.0648	0.5186	-0.4728	1.1689	106.3779	-115.0817	69.7592
138	0.1372	-0.1205	0.0109	0.2149	-0.0767	0.0019	-0.2312	0.2251	-0.0558	-0.0595	0.0724	-0.1073	0.2006	-0.0711	0	0.5099	-0.0186	0.2094	0.7307	-0.595	1.1547	97.8567	-109.1972	44.6081
139	0.067	-0.0476	-0.0289	0.0303	0.0123	0.0012	0.0564	0.1323	-0.116	-0.2192	0.3355	-0.0541	0.1254	0.0696	0	0.9231	0.1814	0.0341	0.7109	-0.6135	1.2349	75.1309	-133.8814	65.9733
140	0.0053	0.0506	0.0475	0.1184	0.121	0.1238	0.0651	-0.0174	-0.1377	0.0425	-0.1384	-0.1579	0.0044	-0.0458	0	0.6327	0.1325	0.0075	0.5852	-0.4885	1.2717	73.0205	-129.2463	72.2721
141	0.035	0.0109	-0.0537	-0.0319	-0.0184	0.1438	-0.2032	0.5851	0.0502	-0.0788	0.6253	-0.4898	0.091	-0.0346	0.0015	0.8031	-0.0933	0.6482	1.2102	-0.3892	1.0843	154.682	7.4523	9.8895
142	0.1459	-0.0857	-0.0773	0.0629	-0.0042	0.1654	0.0443	0.4203	0.2785	-0.2088	-0.2324	-0.5687	-0.1486	0.2073	-0.0135	0.9903	-0.1209	0.6454	1.489	-0.2691	0.688	133.972	12.977	-6.7737
143	0.0115	0.0178	-0.0249	0.0247	-0.0325	0.0307	-0.3872	-0.0224	0.1575	0.2249	-0.1271	-0.1663	-0.0481	-0.2224	-0	1.111	0.1154	0.7479	1.6671	-0.4301	0.9912	149.8617	-23.4258	-9.1798
144	0.0043	-0.0111	-0.001	0.0703	0.1214	0.1595	0.3371	0.2708	0.0117	0.1451	-0.1004	-0.4205	0.2755	-0.1198	0.0035	0.9281	-0.1703	0.8131	1.4679	-0.5474	1.1904	148.5158	-26.3657	-1.7622
145	0.0228	0.0247	-0.0368	0.2376	-0.1389	0.051	-0.0948	0.3691	-0.0615	-0.3188	0.2129	-0.619	0.1888	-0.2407	0.0008	0.5205	0.1126	0.5214	1.0045	-0.5625	1.5996	165.4031	-49.052	39.164
146	0.0905	-0.0612	-0.0955	0.2218	-0.0769	0.1615	0.0357	-0.0127	-0.5107	-0.1922	0.1137	-0.7151	-0.3157	-0.0215	0	0.5239	0.0335	0.501	1.0404	-0.3546	1.3816	169.0248	-24.0655	29.1044
147	-0.0062	0.0124	-0.0282	0.0317	-0.0536	0.0715	0.1683	0.0324	0.0424	0.2248	0.1602	-0.1104	-0.2544	-0.0838	-0	0.8759	-0.0611	0.6278	1.4456	-0.5782	1.4788	153.8156	-51.2629	4.4514
148	0.0667	0.0151	-0.0895	-0.0395	0.0122	0.1386	0.106	0.0911	-0.6404	-0.4802	0.242	-0.8325	0.0966	-0.1845	0.0025	0.7348	0.0364	0.5997	1.3536	-0.6851	1.5356	146.9137	-53.285	8.1749
149	0.2786	0.0201	0.1553	0.1061	-0.0498	0.0576	-0.0811	0.2139	-0.1553	-0.267	0.003	-0.3828	0.0329	-0.2357	0	0.5154	-0.0093	0.4074	1.0319	-0.6753	1.148	115.9978	-88.3818	25.446
150	0.1882	0.1018	0.043	0.0914	-0.088	0.1038	0.2659	0.0168	-0.215	0.0485	0.0854	-0.1902	-0.0236	0.0934	0	0.5414	0.0538	0.4359	1.0401	-0.5913	1.411	140.0808	-79.1503	34.0575
151	0.0462	-0.0258	0.027	0.0248	0.0139	0.0193	0.0347	0.3354	-0.1641	-0.001	0.101	0.1653	0.3147	0.2077	-0	0.8175	0.0012	0.6242	1.5647	-0.9156	1.4936	129.3014	-69.2754	-2.9217
152	-0.0183	0.0152	-0.0001	0.0685	0.1249	0.1347	0.0378	-0.0025	0.0576	-0.069	0.301	-0.239	-0.2096	-0.041	-0	0.7259	-0.0051	0.5964	1.3375	-0.7969	1.2769	122.5381	-65.0087	-1.6497
153	0.2803	0.0923	0.1854	0.1468	0.099	0.1531	0.2647	-0.0547	-0.3112	-0.1258	0.157	-0.3818	0.249	0.1417	0.0217	0.9305	-0.0086	0.4724	1.3277	-0.6782	0.4467	74.7102	-55.9995	-12.2705
154	0.1017	-0.0207	-0.0765	0.1116	-0.1582	0.223	-0.2704	-0.0315	-0.1784	-0.7948	0.2865	-0.6405	-0.0207	-0.054	0	0.7707	0.0367	0.4386	1.3145	-0.6513	0.8009	87.1246	-76.1569	1.1474
155	0.0149	0.0004	0.027	0.0114	0.0239	0.0347	-0.0232	-0.0868	-0.135	-0.0734	0.4222	0.0835	0.1914	-0.0898	-0	1.1087	-0.0043	0.6664	1.5398	-0.5612	0.8726	110.0817	-52.5686	-21.2089
156	0.0577	0.0835	0.0054	0.0695	0.0712	-0.0186	-0.0701	0.1088	-0.0223	-0.5904	0.0525	-0.3075	0.1131	-0.0116	0	1.024	0.0003	0.6109	1.6496	-0.5972	0.9071	108.9967	-45.3347	-17.7355
157	-0.0018	0.0347	0.0026	0.1619	-0.0532	0.0062	-0.0408	0.0107	-0.1636	-0.3622	0.3104	-0.4058	0.0806	0.0344	0.0007	1.2482	-0.1519	0.6601	1.5444	-0.1796	0.521	98.6533	3.2425	-21.8374
158	0.1358	-0.1128	-0.1035	0.1237	0.1018	0.0642	0.1319	0.415	0.1263	-0.4261	-0.0179	-0.4044	0.1221	-0.0315	-0.0014	1.2282	-0.1733	0.6457	1.4831	-0.4126	0.4453	83.3707	-19.1661	-24.0713
159	0.0196	0.0373	-0.0057	0.0338	-0.0027	0.0147	0.1517	-0.0532	0.0144	-0.0042	-0.1796	0.1035	0.1164	0.1855	-0	1.2517	-0.3094	0.7194	1.8775	-0.7177	0.8965	122.7604	-24.1991	-25.0684
160	0.028	-0.1299	0.0458	0.4094	0.005	0.0759	-0.0632	0.2585	-0.1873	0.4309	0.089	-0.3139	0.0805	0.0121	-0.0042	1.2125	-0.164	0.7595	1.6194	-0.4706	0.8423	125.0205	-21.4444	-17.7966
161	0.4975	0.0807	0.152	0.0327	0.0532	0.0768	0.0683	0.28	0.3553	-0.2037	0.0468	-0.0233	0.0571	0.1871	-0.0133	1.1839	-0.0879	0.3115	1.6848	0.2705	0.1791	57.1052	35.5244	-20.2127
162	0.2119	0.1548	-0.0182	0.245	-0.217	0.2337	0.0905	0.4675	-0.0628	-0.059	-0.1369	0.0917	0.0223	-0.0766	0.0005	1.189	-0.1223	0.4941	1.5354	0.168	0.2593	84.1975	33.5836	-20.8569
163	0.0638	0.0057	-0.0514	-0.0081	-0.0129	0.0312	0.1779	-0.0233	-0.0259	-0.0397	0.0705	-0.2041	0.3113	-0.0345	-0	1.1683	-0.0491	0.3747	1.3284	0.368	0.4216	68.9206	70.303	-19.8858
164	0.2582	0.1855	0.1132	0.3529	-0.0293	0.0866	0.079	0.3459	0.247	-0.2387	-0.1609	0.0345	-0.2757	-0.008	-0.0606	1.3942	-0.1719	0.395	1.6299	0.4105	0.26	64.9273	70.3003	-12.8426
165	0.1275	-0.0781	-0.0365	0.0245	0.074	0.0119	-0.0374	0.3706	-0.0684	-0.0183	0.0184	0.1612	0.0362	0.1028	-0.2253	0.9997	0.1328	0.1536	1.2478	0.6036	0.154	23.348	79.3308	13.1818
166	0.2616	-0.2299	-0.1103	0.5367	-0.1174	0.1654	-0.1288	0.3991	-0.159	-0.2533	0.0546	0.3166	-0.2491	-0.0053	-0.0079	1.064	0.017	0.1421	1.3208	0.3518	0.1413	30.0301	60.0163	-4.7424
167	0.3558	0.2883	0.1132	0.2792	0.0435	0.1302	-0.2463	-0.0022	0.1831	0.1399	-0.1142	0.1364	0.1638	0.2245	-0.0543	1.0588	0.0399	0.1038	1.0929	0.6312	0.3417	53.6342	91.9876	-3.1541
168	0.1873	-0.1521	-0.1108	0.2108	-0.0468	0.2683	-0.1203	-0.0392	0.2966	-0.2036	0.4491	-0.0913	-0.0071	0.2433	0.0462	1.0863	-0.1229	0.213	1.4756	0.6061	0.2254	56.3894	91.6872	4.4513
169	0.1449	0.1688	-0.017	0.1883	-0.0541	0.3287	0.1535	0.3196	0.12	-0.0845	-0.1192	0.218	-0.2511	0.1327	-0.0013	0.8169	0.0343	0.1782	0.8861	0.6724	0.7161	64.8457	114.3916	47.9798
170	0.9333	0.2305	-0.1303	0.182	-0.1357	0.1609	-0.0351	-0.0722	0.8883	-0.0572	-0.1075	0.2191	-0.0267	-0.1748	-0.0447	0.6484	0.0773	0.0838	0.7342	0.9178	-0.103	42.0882	105.9049	35.7526
171	0.1829	-0.1502	0.0059	0.1778	-0.0179	0.1653	0.3361	-0.1283	0.2136	0.0448	0.0802	-0.0262	-0.1398	0.1714	0.0282	0.9475	-0.0989	0.1118	1.2921	0.839	0.5107	74.7555	108.228	13.2154
172	-0.0011	0.0384	-0.0723	0.0526	-0.1342	0.2423	0.1579	0.2124	0.001	-0.1543	0.3027	-0.193	0.2768	0.3463	0.0092	1.0625	-0.0076	0.2654	1.388	0.6604	0.7297	79.7225	102.9685	16.863
173	0.1107	0.0873	-0.1499	0.095	-0.141	0.061	0.0427	0.0581	0.1778	-0.2849	0.0261	-0.1708	-0.038	0.0177	0	0.7143	-0.0665	0.4053	0.9704	0.4448	0.8172	124.3414	92.0904	36.3429
174	0.162	0.1233	-0.2165	0.0583	-0.0754	0.2239	0.0628	0.0946	-0.0455	0.0315	0.4514	-0.2512	-0.1598	-0.1859	0.0021	0.7555	-0.0146	0.2985	0.9858	0.5327	0.7737	103.8398	107.7936	44.8468
175	0.0251	-0.0548	-0.0154	0.0771	0.016	-0.0001	-0.0498	-0.1011	-0.062	-0.1369	0.0676	0.201	-0.0056	-0.1095	-0	1.2292	0.0638	0.5865	1.0781	0.5953	0.8121	103.1426	96.5206	6.7195
176	0.2876	-0.0173	0.1778	0.2343	-0.0178	0.2667	-0.1833	0.345	-0.6492	-0.1936	0.1768	-0.1215	-0.2435	0.1925	0.0396	1.0375	-0.0713	0.5594	1.2817	0.5808	0.776	102.714	88.4594	7.331
177	0.0785	0.0955	0.0023	-0.0007	0.0454	-0.0293	0.2234	0.1996	0.1361	-0.3728	-0.0075	-0.0634	-0.1961	0.2087	0.0001	1.158	-0.1276	0.5836	1.4064	0.1473	0.6626	119.504	43.3419	-5.8608
178	-0.0129	-0.0017	0.0252	0.0203	-0.0967	0.4208	-0.0552	0.393	0.0297	0.0417	0.122	-0.0188	-0.2258	0.2115	-0	0.8288	-0.153	0.5278	1.1672	0.3371	0.8843	129.8348	62.9017	9.9735
179	0.0086	0.0146	-0.0239	0.0266	-0.0116	0.0194	0.0318	0.2636	-0.1581	0.1731	-0.0776	-0.0002	0.0905	0.0339	-0	1.5108	-0.2397	0.4559	1.6364	0.283	0.7777	99.5248	73.091	-13.656
180	0.2177	-0.2985	-0.0388	0.5608	-0.1545	0.1058	0.2024	0.4233	-0.1209	-0.1814	-0.1764	0.38	-0.0691	0.0271	0.0171	1.1393	-0.1367	0.5867	1.298	0.453	0.4857	93.582	68.2827	-10.9814
181	0.1114	-0.1073	-0.0762	0.0524	0.0483	0.0316	0.0219	-0.003	-0.1441	0.2812	0.1051	-0.057	-0.21	0.0612	0.0005	0.6702	-0.1549	-0.4592	0.4038	0.0585	0.5813	96.1428	-11.6279	220.3867
182	0.3246	-0.0727	0.2775	0.0227	-0.1019	0.1581	-0.2257	-0.1972	-0.0021	0.5266	0.0631	-0.1666	-0.0311	-0.1144	-0.0029	0.6991	-0.1297	-0.436	0.3932	-0.0513	0.4947	87.7098	14.1389	222.7838
183	0.0337	-0.0689	-0.0408	0.111	0.082	0.0362	0.0337	-0.1049	-0.1195	-0.2776	-0.0076	-0.0406	-0.2089	0.0563	-0	0.923	-0.1431	-0.5968	0.3982	-0.0735	0.715	126.904	7.8839	223.631
184	0.1981	-0.0178	0.1027	0.1261	-0.0719	0.0189	-0.151	-0.3556	-0.1796	-0.0324	0.0932	-0.3206	0.2662	-0.0244	-0.006	0.7605	-0.1283	-0.6955	0.4148	0.0123	0.8516	128.2857	4.6809	216.3221
185	-0.0164	0.0024	-0.0174	-0.0051	0.0403	0.0484	0.0228	-0.1872	-0.3997	-0.0417	0.1042	-0.243	-0.0348	0.1137	0.002	0.5125	-0.0293	-0.6461	0.3698	0.085	1.1949	148.6936	-31.1621	188.4588
186	0.1454	-0.0273	0.0156	0.0716	0.1185	0.1978	0.0139	-0.0994	-0.0766	0.3058	-0.2596	-0.1413	0.0262	-0.0173	0	0.6226	-0.0749	-0.6702	0.4416	0.0551	1.0762	127.2038	-30.6841	205.1238
187	0.0009	-0.0222	0.0271	0.0562	-0.0573	0.0341	0.0345	0.1477	-0.0194	-0.2694	0.1091	0.0294	0.3753	0.0102	-0	0.6318	-0.0777	-0.5699	0.463	0.2068	1.1433	152.6893	-0.3678	207.8214
188	0.045	-0.0096	-0.0346	0.3198	0.1165	0.0551	0.2177	-0.3523	-0.0515	-0.3693	-0.1649	-0.6381	-0.1357	-0.0597	-0.0047	0.6704	-0.1011	-0.6412	0.3988	0.0877	1.2259	152.2666	2.9004	200.4329
189	-0.0495	0.0324	-0.0043	0.1595	0.0305	-0.1193	0.1634	0.1448	-0.0251	0.0799	0.0307	-0.3365	-0.1103	-0.129	0.0006	0.3479	0.0439	-0.3985	0.3284	-0.0326	1.5224	174.9937	20.0095	159.498
190	0.136	0.1657	0.1062	0.2089	0.0965	0.0281	-0.0455	-0.1162	0.107	0.1183	0.0046	-0.2538	0.3124	0.0661	-0	0.4798	-0.0048	-0.4582	0.4395	0.0201	1.3821	171.472	-5.0078	169.5099
191	0.0486	0.0982	-0.0425	0.1952	-0.1167	0.1325	0.1957	-0.2499	0.2473	-0.0937	-0.0793	-0.0709	0.3385	-0.1258	-0.0075	0.4473	-0.1039	-0.6763	0.309	-0.074	1.49	164.4157	25.3141	194.1994
192	0.1602	-0.1324	0.0002	0.2187	0.2645	0.3527	0.3901	-0.1136	0.1879	0.0057	-0.0955	-0.471	-0.2605	-0.1509	0.0184	0.5123	-0.1095	-0.5743	0.3064	0.0846	1.3584	158.3573	29.1829	190.474
193	0.0906	0.1698	-0.0607	0.0399	0.1271	0.5032	-0.0033	-0.1326	0.1336	0.0726	0.3262	-0.3333	-0.1957	-0.2375	0.0002	0.4595	0.0838	-0.2874	0.3702	-0.0194	1.01	138.1742	71.1235	172.8902
194	0.2083	-0.0103	0.1133	-0.0078	0.0341	0.2271	0.1119	0.193	0.0279	0.1173	-0.1135	-0.3806	-0.0029	0.2093	-0	0.3368	0.0113	-0.2966	0.3133	0.0963	1.1531	158.994	55.7676	164.4841
195	0.148	0.062	-0.0071	0.1407	-0.2466	0.5532	0.6351	-0.0928	-0.2943	0.2432	0.1924	-0.0248	0.0285	-0.0813	0.07	0.609	-0.164	-0.5125	0.4151	-0.1099	0.9315	145.6067	49.3191	201.3957
196	0.0316	0.0136	0.1198	0.1833	0.1724	0.1907	0.2214	-0.0012	0.0357	0.2375	0.079	-0.213	0.0155	0.0027	0.0108	0.5325	-0.1106	-0.4921	0.2939	-0.0733	0.947	138.0077	47.0204	200.0751
197	0.2173	0.2663	-0.0856	0.1717	-0.0595	0.2009	0.2255	-0.3242	-0.1934	0.1051	-0.1342	-0.1682	0.0165	0.0015	0	0.5239	-0.1975	-0.3047	0.3046	-0.0536	0.4957	89.7252	51.8513	210.801
198	0.4163	-0.0832	0.2535	0.0961	-0.1451	0.2593	0.1165	0.2857	0.3484	0.5864	-0.2549	-0.3123	0.0132	0.0954	-0.0008	0.4825	-0.1851	-0.321	0.434	-0.0475	0.7388	107.2704	67.489	197.1138
199	0.1799	-0.022	-0.009	0.4597	-0.1867	0.2071	-0.0481	0.1895	0.1441	0.6465	0.2059	-0.2383	0.1172	-0.1467	0.0508	0.8682	-0.2155	-0.6626	0.5611	-0.1039	0.7714	122.7225	38.5942	219.6698
200	0.1823	-0.0264	0.1186	0.1953	-0.1942	0.0954	0.0003	-0.0249	-0.2637	0.1336	0.0704	-0.067	0.1704	0.1437	-0	0.6036	-0.1259	-0.4513	0.383	-0.1427	0.7986	119.6083	31.933	216.2835
201	0.1109	-0.197	-0.0542	0.2247	0.0425	0.0001	-0.0636	0.0503	-0.2247	-0.098	0.1219	-0.372	-0.1952	0.2205	-0	0.2794	-0.011	0.0058	0.5676	-0.1061	1.8081	191.6466	2.6334	112.6445
202	0.3262	-0.0241	-0.1531	0.0717	-0.1139	0.1824	-0.043	0.0585	-0	0.038	0.1928	-0.4363	0.2924	0.1479	0	0.2143	0.0012	-0.1392	0.4685	0.0016	1.7459	187.2329	24.3163	128.4323
203	0.0346	0.0055	0.0606	0.0165	0.0383	0.1096	0.4289	-0.1941	-0.1932	-0.0285	-0.3392	0.2023	0.1469	-0.0447	-0	0.2146	0.007	0.1366	0.8908	-0.1596	1.92	201.8204	31.2906	92.0955
204	0.2255	0.2276	0.0008	0.1033	-0.0268	-0.0102	0.1395	0.1061	-0.1151	0.1203	-0.061	-0.2384	0.0868	0.0364	-0	0.2507	-0.0438	0.0934	0.6637	-0.099	1.7018	195.9659	28.3824	87.3183
205	0.1899	-0.1275	0.1619	0.0555	-0.1121	0.0762	-0.087	-0.1455	-0.0874	-0.0261	-0.0449	-0.1879	0.0581	-0.0077	-0	0.5068	-0.0161	0.427	1.0623	-0.203	1.4923	181.9036	-0.0016	48.831
206	0.008	-0.0258	0.0243	-0.0058	-0.055	0.362	0.0506	0.202	-0.118	-0.0246	0.0588	-0.3263	0.2017	-0.0463	-0	0.425	0.023	0.1973	0.8373	-0.2285	1.801	190.4883	-5.959	73.9615
207	0.0508	0.0261	0.0724	0.0343	0.044	0.0865	0.2941	-0.148	-0.2888	0.1246	-0.2804	-0.0176	-0.0262	-0.1104	-0	0.5696	-0.0371	0.49	1.0331	0.0068	1.5725	196.6183	31.2183	61.2176
208	0.1027	0.0385	0.0586	0.0055	0.0128	0.0071	-0.1647	0.1817	-0.051	-0.2957	-0.1385	0.1804	-0.0653	-0.1536	-0.0008	0.312	-0.1176	0.4047	0.851	-0.2263	1.4253	189.068	33.8527	59.9346
209	0.079	-0.0378	-0.1269	0.0924	-0.0209	0.0491	-0.3033	0.1967	0.0314	-0.1958	0.1267	-0.3999	0.1967	0.1233	-0.0055	0.6248	-0.1649	0.6102	0.9962	0.1258	1.073	155.6619	55.9834	30.3855
210	0.1366	0.2182	-0.0716	0.2217	-0.108	0.0244	0.2672	0.0378	0.0257	-0.4974	0.1569	-0.7092	-0.457	-0.0808	-0	0.6075	-0.0829	0.6184	1.0079	-0.062	1.1589	167.5	31.4986	29.7657
211	-0.0031	0.0097	-0.013	0.0159	-0.0221	0.0137	0.1237	0.2648	-0.4117	0.0862	0.2355	0.0463	0.0709	0.1906	-0	0.5029	-0.121	0.3728	0.9473	-0.0216	1.2977	183.9124	58.7962	53.4676
212	0.0984	0.0612	0.0695	-0.0015	0.0514	0.0177	-0.0055	0.1742	0.1959	0.1527	0.1158	-0.1873	-0.0635	0.0099	-0	0.4319	-0.0509	0.471	0.8873	0.1885	1.5474	177.921	60.3527	58.691
213	-0.0103	0.038	-0.0366	0.0897	-0.1871	0.157	-0.0455	-0.0144	0.1093	-0.3494	0.2948	-0.2644	-0.0975	-0.0179	-0	0.4291	-0.0255	0.239	0.744	0.244	1.041	149.1975	93.3011	82.6722
214	0.0524	0.0992	0.0876	0.1131	0.1008	0.0813	-0.1461	0.1174	0.043	-0.2612	0.1377	-0.285	-0.2143	0.0927	0	0.5185	-0.0575	0.366	0.8549	0.3847	1.1376	150.0795	85.0453	56.7954
215	0.0923	-0.0504	-0.0034	0.1091	-0.0639	0.0338	-0.4967	-0.0753	0.0726	0.0954	0.0445	-0.164	-0.0555	-0.2962	-0.0034	0.4529	-0.0935	0.3857	0.7773	0.2346	1.311	181.3323	75.8799	79.6249
216	0.0736	0.0619	-0.0353	0.2041	-0.1393	0.0234	-0.3445	0.1743	-0.1969	0.0282	0.2253	-0.1796	0.1337	0.073	-0	0.4346	-0.0325	0.2152	0.7873	0.1046	1.5247	177.9719	71.2355	85.3412
217	-0.0038	0.1471	-0.1195	0.2854	-0.4132	0.3751	-0.2205	0.0808	-0.0161	-0.0279	0.0928	-0.1557	-0.0042	0.0456	-0	0.2537	-0.0568	-0.1416	0.3689	0.0901	1.3337	171.3376	60.2199	133.5166
218	0.5245	0.2704	-0.1428	0.1052	-0.1247	0.0589	0.0663	0.0735	0.2084	0.0659	0.1631	-0.6352	-0.0353	-0.167	0	0.4211	0.0141	0.0273	0.5181	0.26	1.3944	162.2086	80.4866	117.8435
219	0.0299	0.0365	-0.023	0.0826	-0.1252	0.1061	-0.137	-0.0579	-0.0628	-0.1065	0.4461	-0.1054	0.2495	-0.0356	-0	0.2714	-0.0912	0.1192	0.6194	0.1496	1.5852	192.3727	58.876	103.5968
220	0.1125	0.1052	-0.1696	0.0637	-0.0819	0.0992	-0.1849	0.2383	-0.1156	-0.064	0.201	-0.2973	0.5216	-0.11	0	0.369	-0.0802	0.0148	0.6312	0.0829	1.4464	189.1051	51.4821	103.1083
221	0.0911	-0.1252	0.0152	0.1058	0.0389	-0.0283	0.2487	0.2615	0.3013	0.1265	-0.2555	-0.0096	-0.1814	-0.0158	-0.0022	0.5361	0.018	0.0993	0.2574	0.052	0.6755	36.5785	106.7658	156.8126
222	0.1285	0.1175	0.1844	0.1517	-0.0248	0.3908	-0.2548	0.1103	0.2319	-0.1811	0.062	0.2085	0.1365	-0.0821	-0	0.4165	0.0599	0.0487	0.3392	0.2311	0.6147	30.3299	115.9461	131.959
223	0.0606	-0.0945	0.0161	0.0849	-0.0189	0.0004	-0.0773	-0.2099	0.2597	-0.0611	0.1978	0.4733	-0.0416	-0.0591	0	0.701	0.0008	0.0268	0.4469	0.0328	0.9741	64.0573	129.3798	148.1158
224	0.1223	0.1226	-0.028	0.0793	0.0158	-0.0531	0.2426	-0.0175	0.1011	-0.0164	-0.2252	-0.0527	-0.0024	0.0663	-0	0.6346	-0.0134	0.1442	0.2465	0.2114	0.975	68.3291	122.5629	149.0683
225	0.3233	-0.3733	-0.1483	0.2694	0.0361	-0.0468	-0.037	-0.107	0.4287	0.0155	-0.273	-0.3684	0.0658	-0.1332	-0.0017	0.5031	-0.143	-0.1825	0.2891	0.0895	0.8873	95.8439	92.657	177.8752
226	0.0676	0.0475	0.0145	0.2645	0.2086	0.1305	0.0691	-0.1747	0.1819	0.2625	-0.1219	-0.0029	-0.2588	-0.0143	-0	0.5664	-0.0683	-0.0654	0.2393	-0.0015	0.7628	69.2816	98.5241	177.4381
227	0.0845	-0.0933	-0.0647	0.0809	0.0609	0.0374	0.1237	0.0293	-0.0077	0.0259	-0.0877	0.1197	-0.3242	0.2141	-0	0.6021	-0.018	-0.0214	0.3737	0.0148	1.0231	93.3098	122.7897	157.1084
228	0.1211	-0.0328	-0.1729	0.0989	0.0994	0.1352	0.3988	-0.0342	0.387	0.3286	-0.2797	-0.1704	-0.2619	0.1597	-0	0.5633	0.011	-0.0235	0.2071	0.1126	1.0065	96.5326	117.7927	151.611
229	0.0151	-0.1189	-0.1044	0.0726	0.1644	0.1854	0.0803	-0.004	0.3431	0.0854	-0.1405	-0.4284	-0.1394	-0.0817	-0	0.5127	-0.015	0.0822	0.3913	0.1867	1.1338	136.8253	99.7321	128.6153
230	0.1009	-0.0486	-0.065	0.5136	0.1977	0.0574	-0.1083	-0.0342	0.0768	0.0136	0.0609	-0.1469	-0.1211	0.067	-0	0.399	-0.0347	-0.0647	0.1957	0.0868	1.1074	126.7752	96.283	153.6117
231	0.0792	-0.037	0.0163	0.0319	0.0318	0.0649	0.0369	0.4984	-0.1762	-0.1303	-0.25	0.1114	0.0328	-0.0107	0.0006	0.7183	-0.0552	0.0179	0.2973	0.316	1.1848	112.1926	126.6172	132.343
232	-0.0089	0.0054	0.0332	0.2136	0.1433	0.0842	0.1331	0.1681	0.2232	0.2223	-0.1495	0.1477	-0.1881	0.0017	0	0.4661	-0.0503	0.0857	0.3834	0.2078	1.0309	108.8906	122.8246	126.0041
233	0.1225	-0.0846	0.0163	0.0178	-0.0473	0.0226	-0.0538	0.1637	0.0123	-0.2382	-0.092	-0.047	0.0324	-0.0999	-0	0.5572	0.016	0.176	0.538	0.4309	0.9583	103.032	118.0811	76.8338
234	0.0179	0.0144	0.0509	0.5204	0.0633	0.0543	0.0742	0.2313	0.4392	0.1149	0.1252	-0.1861	0.0316	0.1725	0	0.4681	0.0042	0.0715	0.5625	0.3165	0.9048	123.8005	112.5696	93.5281
235	0.0109	0.013	0.0318	0.0616	0.0857	0.0905	-0.0025	-0.235	0.3172	-0.1131	0.0176	-0.0457	0.2073	-0.4114	0	0.7381	-0.0067	0.09	0.4529	0.393	1.1646	94.7294	135.4655	107.9842
236	0.0137	0.0931	-0.0873	0.2573	0.0045	0.0923	0.0109	0.1721	0.2655	-0.0057	-0.1563	0.0902	-0.0363	-0.3622	-0.0022	0.5004	0.0251	0.0602	0.3465	0.3533	0.8081	88.3085	130.5458	107.5893
237	0.0292	-0.1513	-0.0684	0.0539	0.0275	-0.0011	0.2848	0.0633	0.4463	0.1615	-0.1186	0.0896	0.1079	0.016	-0.0005	0.5504	0.0895	0.1081	0.4323	0.4191	0.7664	40.9498	122.4314	94.2117
238	0.0055	-0.0319	-0.0948	0.3463	0.3733	0.2907	-0.0301	0.4421	0.5686	-0.039	0.0982	-0.0823	-0.1886	0.3205	0	0.641	0.0473	0.11	0.638	0.4786	0.6852	64.0364	124.5898	80.0221
239	0.0644	0.0416	0.0282	0.0695	-0.0513	0.0779	-0.1529	-0.0206	-0.1257	-0.1211	0.0422	0.2985	-0.2095	0.3193	-0	0.8096	0.1655	0.1184	0.4429	0.1972	1.2292	64.906	137.1661	117.7275
240	0.0318	0.0507	0.0934	0.1636	0.1737	0.1522	0.2041	0.0623	0.3317	-0.0479	-0.0689	-0.4831	0.0824	-0.1753	0	0.5012	0.0565	0.1745	0.4203	0.3511	0.9844	63.1644	130.3989	121.8329

Refinement TLS group

ID	Refine-ID	Refine TLS-ID	Selection details
1	X-RAY DIFFRACTION	1	(CHAIN AA AND RESID 1:189)
2	X-RAY DIFFRACTION	2	(CHAIN AA AND RESID 190:343)
3	X-RAY DIFFRACTION	3	(CHAIN AA AND RESID 344:384)
4	X-RAY DIFFRACTION	4	(CHAIN AA AND RESID 385:504)
5	X-RAY DIFFRACTION	5	(CHAIN AB AND RESID 1:189)
6	X-RAY DIFFRACTION	6	(CHAIN AB AND RESID 190:343)
7	X-RAY DIFFRACTION	7	(CHAIN AB AND RESID 344:384)
8	X-RAY DIFFRACTION	8	(CHAIN AB AND RESID 385:504)
9	X-RAY DIFFRACTION	9	(CHAIN AC AND RESID 1:189)
10	X-RAY DIFFRACTION	10	(CHAIN AC AND RESID 190:343)
11	X-RAY DIFFRACTION	11	(CHAIN AC AND RESID 344:384)
12	X-RAY DIFFRACTION	12	(CHAIN AC AND RESID 385:504)
13	X-RAY DIFFRACTION	13	(CHAIN AD AND RESID 1:189)
14	X-RAY DIFFRACTION	14	(CHAIN AD AND RESID 190:343)
15	X-RAY DIFFRACTION	15	(CHAIN AD AND RESID 344:384)
16	X-RAY DIFFRACTION	16	(CHAIN AD AND RESID 385:504)
17	X-RAY DIFFRACTION	17	(CHAIN AE AND RESID 1:189)
18	X-RAY DIFFRACTION	18	(CHAIN AE AND RESID 190:343)
19	X-RAY DIFFRACTION	19	(CHAIN AE AND RESID 344:384)
20	X-RAY DIFFRACTION	20	(CHAIN AE AND RESID 385:504)
21	X-RAY DIFFRACTION	21	(CHAIN AF AND RESID 1:189)
22	X-RAY DIFFRACTION	22	(CHAIN AF AND RESID 190:343)
23	X-RAY DIFFRACTION	23	(CHAIN AF AND RESID 344:384)
24	X-RAY DIFFRACTION	24	(CHAIN AF AND RESID 385:504)
25	X-RAY DIFFRACTION	25	(CHAIN AG AND RESID 1:189)
26	X-RAY DIFFRACTION	26	(CHAIN AG AND RESID 190:343)
27	X-RAY DIFFRACTION	27	(CHAIN AG AND RESID 344:384)
28	X-RAY DIFFRACTION	28	(CHAIN AG AND RESID 385:504)
29	X-RAY DIFFRACTION	29	(CHAIN AH AND RESID 1:189)
30	X-RAY DIFFRACTION	30	(CHAIN AH AND RESID 190:343)
31	X-RAY DIFFRACTION	31	(CHAIN AH AND RESID 344:384)
32	X-RAY DIFFRACTION	32	(CHAIN AH AND RESID 385:504)
33	X-RAY DIFFRACTION	33	(CHAIN AI AND RESID 1:189)
34	X-RAY DIFFRACTION	34	(CHAIN AI AND RESID 190:343)
35	X-RAY DIFFRACTION	35	(CHAIN AI AND RESID 344:384)
36	X-RAY DIFFRACTION	36	(CHAIN AI AND RESID 385:504)
37	X-RAY DIFFRACTION	37	(CHAIN AJ AND RESID 1:189)
38	X-RAY DIFFRACTION	38	(CHAIN AJ AND RESID 190:343)
39	X-RAY DIFFRACTION	39	(CHAIN AJ AND RESID 344:384)
40	X-RAY DIFFRACTION	40	(CHAIN AJ AND RESID 385:504)
41	X-RAY DIFFRACTION	41	(CHAIN AK AND RESID 1:189)
42	X-RAY DIFFRACTION	42	(CHAIN AK AND RESID 190:343)
43	X-RAY DIFFRACTION	43	(CHAIN AK AND RESID 344:384)
44	X-RAY DIFFRACTION	44	(CHAIN AK AND RESID 385:504)
45	X-RAY DIFFRACTION	45	(CHAIN AL AND RESID 1:189)
46	X-RAY DIFFRACTION	46	(CHAIN AL AND RESID 190:343)
47	X-RAY DIFFRACTION	47	(CHAIN AL AND RESID 344:384)
48	X-RAY DIFFRACTION	48	(CHAIN AL AND RESID 385:504)
49	X-RAY DIFFRACTION	49	(CHAIN AM AND RESID 1:189)
50	X-RAY DIFFRACTION	50	(CHAIN AM AND RESID 190:343)
51	X-RAY DIFFRACTION	51	(CHAIN AM AND RESID 344:384)
52	X-RAY DIFFRACTION	52	(CHAIN AM AND RESID 385:504)
53	X-RAY DIFFRACTION	53	(CHAIN AN AND RESID 1:189)
54	X-RAY DIFFRACTION	54	(CHAIN AN AND RESID 190:343)
55	X-RAY DIFFRACTION	55	(CHAIN AN AND RESID 344:384)
56	X-RAY DIFFRACTION	56	(CHAIN AN AND RESID 385:504)
57	X-RAY DIFFRACTION	57	(CHAIN AO AND RESID 1:189)
58	X-RAY DIFFRACTION	58	(CHAIN AO AND RESID 190:343)
59	X-RAY DIFFRACTION	59	(CHAIN AO AND RESID 344:384)
60	X-RAY DIFFRACTION	60	(CHAIN AO AND RESID 385:504)
61	X-RAY DIFFRACTION	61	(CHAIN AP AND RESID 1:189)
62	X-RAY DIFFRACTION	62	(CHAIN AP AND RESID 190:343)
63	X-RAY DIFFRACTION	63	(CHAIN AP AND RESID 344:384)
64	X-RAY DIFFRACTION	64	(CHAIN AP AND RESID 385:504)
65	X-RAY DIFFRACTION	65	(CHAIN AQ AND RESID 1:189)
66	X-RAY DIFFRACTION	66	(CHAIN AQ AND RESID 190:343)
67	X-RAY DIFFRACTION	67	(CHAIN AQ AND RESID 344:384)
68	X-RAY DIFFRACTION	68	(CHAIN AQ AND RESID 385:504)
69	X-RAY DIFFRACTION	69	(CHAIN AR AND RESID 1:189)
70	X-RAY DIFFRACTION	70	(CHAIN AR AND RESID 190:343)
71	X-RAY DIFFRACTION	71	(CHAIN AR AND RESID 344:384)
72	X-RAY DIFFRACTION	72	(CHAIN AR AND RESID 385:504)
73	X-RAY DIFFRACTION	73	(CHAIN AS AND RESID 1:189)
74	X-RAY DIFFRACTION	74	(CHAIN AS AND RESID 190:343)
75	X-RAY DIFFRACTION	75	(CHAIN AS AND RESID 344:384)
76	X-RAY DIFFRACTION	76	(CHAIN AS AND RESID 385:504)
77	X-RAY DIFFRACTION	77	(CHAIN AT AND RESID 1:189)
78	X-RAY DIFFRACTION	78	(CHAIN AT AND RESID 190:343)
79	X-RAY DIFFRACTION	79	(CHAIN AT AND RESID 344:384)
80	X-RAY DIFFRACTION	80	(CHAIN AT AND RESID 385:504)
81	X-RAY DIFFRACTION	81	(CHAIN BA AND RESID 1:189)
82	X-RAY DIFFRACTION	82	(CHAIN BA AND RESID 190:343)
83	X-RAY DIFFRACTION	83	(CHAIN BA AND RESID 344:384)
84	X-RAY DIFFRACTION	84	(CHAIN BA AND RESID 385:504)
85	X-RAY DIFFRACTION	85	(CHAIN BB AND RESID 1:189)
86	X-RAY DIFFRACTION	86	(CHAIN BB AND RESID 190:343)
87	X-RAY DIFFRACTION	87	(CHAIN BB AND RESID 344:384)
88	X-RAY DIFFRACTION	88	(CHAIN BB AND RESID 385:504)
89	X-RAY DIFFRACTION	89	(CHAIN BC AND RESID 1:189)
90	X-RAY DIFFRACTION	90	(CHAIN BC AND RESID 190:343)
91	X-RAY DIFFRACTION	91	(CHAIN BC AND RESID 344:384)
92	X-RAY DIFFRACTION	92	(CHAIN BC AND RESID 385:504)
93	X-RAY DIFFRACTION	93	(CHAIN BD AND RESID 1:189)
94	X-RAY DIFFRACTION	94	(CHAIN BD AND RESID 190:343)
95	X-RAY DIFFRACTION	95	(CHAIN BD AND RESID 344:384)
96	X-RAY DIFFRACTION	96	(CHAIN BD AND RESID 385:504)
97	X-RAY DIFFRACTION	97	(CHAIN BE AND RESID 1:189)
98	X-RAY DIFFRACTION	98	(CHAIN BE AND RESID 190:343)
99	X-RAY DIFFRACTION	99	(CHAIN BE AND RESID 344:384)
100	X-RAY DIFFRACTION	100	(CHAIN BE AND RESID 385:504)
101	X-RAY DIFFRACTION	101	(CHAIN BF AND RESID 1:189)
102	X-RAY DIFFRACTION	102	(CHAIN BF AND RESID 190:343)
103	X-RAY DIFFRACTION	103	(CHAIN BF AND RESID 344:384)
104	X-RAY DIFFRACTION	104	(CHAIN BF AND RESID 385:504)
105	X-RAY DIFFRACTION	105	(CHAIN BG AND RESID 1:189)
106	X-RAY DIFFRACTION	106	(CHAIN BG AND RESID 190:343)
107	X-RAY DIFFRACTION	107	(CHAIN BG AND RESID 344:384)
108	X-RAY DIFFRACTION	108	(CHAIN BG AND RESID 385:504)
109	X-RAY DIFFRACTION	109	(CHAIN BH AND RESID 1:189)
110	X-RAY DIFFRACTION	110	(CHAIN BH AND RESID 190:343)
111	X-RAY DIFFRACTION	111	(CHAIN BH AND RESID 344:384)
112	X-RAY DIFFRACTION	112	(CHAIN BH AND RESID 385:504)
113	X-RAY DIFFRACTION	113	(CHAIN BI AND RESID 1:189)
114	X-RAY DIFFRACTION	114	(CHAIN BI AND RESID 190:343)
115	X-RAY DIFFRACTION	115	(CHAIN BI AND RESID 344:384)
116	X-RAY DIFFRACTION	116	(CHAIN BI AND RESID 385:504)
117	X-RAY DIFFRACTION	117	(CHAIN BJ AND RESID 1:189)
118	X-RAY DIFFRACTION	118	(CHAIN BJ AND RESID 190:343)
119	X-RAY DIFFRACTION	119	(CHAIN BJ AND RESID 344:384)
120	X-RAY DIFFRACTION	120	(CHAIN BJ AND RESID 385:504)
121	X-RAY DIFFRACTION	121	(CHAIN BK AND RESID 1:189)
122	X-RAY DIFFRACTION	122	(CHAIN BK AND RESID 190:343)
123	X-RAY DIFFRACTION	123	(CHAIN BK AND RESID 344:384)
124	X-RAY DIFFRACTION	124	(CHAIN BK AND RESID 385:504)
125	X-RAY DIFFRACTION	125	(CHAIN BL AND RESID 1:189)
126	X-RAY DIFFRACTION	126	(CHAIN BL AND RESID 190:343)
127	X-RAY DIFFRACTION	127	(CHAIN BL AND RESID 344:384)
128	X-RAY DIFFRACTION	128	(CHAIN BL AND RESID 385:504)
129	X-RAY DIFFRACTION	129	(CHAIN BM AND RESID 1:189)
130	X-RAY DIFFRACTION	130	(CHAIN BM AND RESID 190:343)
131	X-RAY DIFFRACTION	131	(CHAIN BM AND RESID 344:384)
132	X-RAY DIFFRACTION	132	(CHAIN BM AND RESID 385:504)
133	X-RAY DIFFRACTION	133	(CHAIN BN AND RESID 1:189)
134	X-RAY DIFFRACTION	134	(CHAIN BN AND RESID 190:343)
135	X-RAY DIFFRACTION	135	(CHAIN BN AND RESID 344:384)
136	X-RAY DIFFRACTION	136	(CHAIN BN AND RESID 385:504)
137	X-RAY DIFFRACTION	137	(CHAIN BO AND RESID 1:189)
138	X-RAY DIFFRACTION	138	(CHAIN BO AND RESID 190:343)
139	X-RAY DIFFRACTION	139	(CHAIN BO AND RESID 344:384)
140	X-RAY DIFFRACTION	140	(CHAIN BO AND RESID 385:504)
141	X-RAY DIFFRACTION	141	(CHAIN BP AND RESID 1:189)
142	X-RAY DIFFRACTION	142	(CHAIN BP AND RESID 190:343)
143	X-RAY DIFFRACTION	143	(CHAIN BP AND RESID 344:384)
144	X-RAY DIFFRACTION	144	(CHAIN BP AND RESID 385:504)
145	X-RAY DIFFRACTION	145	(CHAIN BQ AND RESID 1:189)
146	X-RAY DIFFRACTION	146	(CHAIN BQ AND RESID 190:343)
147	X-RAY DIFFRACTION	147	(CHAIN BQ AND RESID 344:384)
148	X-RAY DIFFRACTION	148	(CHAIN BQ AND RESID 385:504)
149	X-RAY DIFFRACTION	149	(CHAIN BR AND RESID 1:189)
150	X-RAY DIFFRACTION	150	(CHAIN BR AND RESID 190:343)
151	X-RAY DIFFRACTION	151	(CHAIN BR AND RESID 344:384)
152	X-RAY DIFFRACTION	152	(CHAIN BR AND RESID 385:504)
153	X-RAY DIFFRACTION	153	(CHAIN BS AND RESID 1:189)
154	X-RAY DIFFRACTION	154	(CHAIN BS AND RESID 190:343)
155	X-RAY DIFFRACTION	155	(CHAIN BS AND RESID 344:384)
156	X-RAY DIFFRACTION	156	(CHAIN BS AND RESID 385:504)
157	X-RAY DIFFRACTION	157	(CHAIN BT AND RESID 1:189)
158	X-RAY DIFFRACTION	158	(CHAIN BT AND RESID 190:343)
159	X-RAY DIFFRACTION	159	(CHAIN BT AND RESID 344:384)
160	X-RAY DIFFRACTION	160	(CHAIN BT AND RESID 385:504)
161	X-RAY DIFFRACTION	161	(CHAIN CA AND RESID 1:189)
162	X-RAY DIFFRACTION	162	(CHAIN CA AND RESID 190:343)
163	X-RAY DIFFRACTION	163	(CHAIN CA AND RESID 344:384)
164	X-RAY DIFFRACTION	164	(CHAIN CA AND RESID 385:504)
165	X-RAY DIFFRACTION	165	(CHAIN CB AND RESID 1:189)
166	X-RAY DIFFRACTION	166	(CHAIN CB AND RESID 190:343)
167	X-RAY DIFFRACTION	167	(CHAIN CB AND RESID 344:384)
168	X-RAY DIFFRACTION	168	(CHAIN CB AND RESID 385:504)
169	X-RAY DIFFRACTION	169	(CHAIN CC AND RESID 1:189)
170	X-RAY DIFFRACTION	170	(CHAIN CC AND RESID 190:343)
171	X-RAY DIFFRACTION	171	(CHAIN CC AND RESID 344:384)
172	X-RAY DIFFRACTION	172	(CHAIN CC AND RESID 385:504)
173	X-RAY DIFFRACTION	173	(CHAIN CD AND RESID 1:189)
174	X-RAY DIFFRACTION	174	(CHAIN CD AND RESID 190:343)
175	X-RAY DIFFRACTION	175	(CHAIN CD AND RESID 344:384)
176	X-RAY DIFFRACTION	176	(CHAIN CD AND RESID 385:504)
177	X-RAY DIFFRACTION	177	(CHAIN CE AND RESID 1:189)
178	X-RAY DIFFRACTION	178	(CHAIN CE AND RESID 190:343)
179	X-RAY DIFFRACTION	179	(CHAIN CE AND RESID 344:384)
180	X-RAY DIFFRACTION	180	(CHAIN CE AND RESID 385:504)
181	X-RAY DIFFRACTION	181	(CHAIN CF AND RESID 1:189)
182	X-RAY DIFFRACTION	182	(CHAIN CF AND RESID 190:343)
183	X-RAY DIFFRACTION	183	(CHAIN CF AND RESID 344:384)
184	X-RAY DIFFRACTION	184	(CHAIN CF AND RESID 385:504)
185	X-RAY DIFFRACTION	185	(CHAIN CG AND RESID 1:189)
186	X-RAY DIFFRACTION	186	(CHAIN CG AND RESID 190:343)
187	X-RAY DIFFRACTION	187	(CHAIN CG AND RESID 344:384)
188	X-RAY DIFFRACTION	188	(CHAIN CG AND RESID 385:504)
189	X-RAY DIFFRACTION	189	(CHAIN CH AND RESID 1:189)
190	X-RAY DIFFRACTION	190	(CHAIN CH AND RESID 190:343)
191	X-RAY DIFFRACTION	191	(CHAIN CH AND RESID 344:384)
192	X-RAY DIFFRACTION	192	(CHAIN CH AND RESID 385:504)
193	X-RAY DIFFRACTION	193	(CHAIN CI AND RESID 1:189)
194	X-RAY DIFFRACTION	194	(CHAIN CI AND RESID 190:343)
195	X-RAY DIFFRACTION	195	(CHAIN CI AND RESID 344:384)
196	X-RAY DIFFRACTION	196	(CHAIN CI AND RESID 385:504)
197	X-RAY DIFFRACTION	197	(CHAIN CJ AND RESID 1:189)
198	X-RAY DIFFRACTION	198	(CHAIN CJ AND RESID 190:343)
199	X-RAY DIFFRACTION	199	(CHAIN CJ AND RESID 344:384)
200	X-RAY DIFFRACTION	200	(CHAIN CJ AND RESID 385:504)
201	X-RAY DIFFRACTION	201	(CHAIN CK AND RESID 1:189)
202	X-RAY DIFFRACTION	202	(CHAIN CK AND RESID 190:343)
203	X-RAY DIFFRACTION	203	(CHAIN CK AND RESID 344:384)
204	X-RAY DIFFRACTION	204	(CHAIN CK AND RESID 385:504)
205	X-RAY DIFFRACTION	205	(CHAIN CL AND RESID 1:189)
206	X-RAY DIFFRACTION	206	(CHAIN CL AND RESID 190:343)
207	X-RAY DIFFRACTION	207	(CHAIN CL AND RESID 344:384)
208	X-RAY DIFFRACTION	208	(CHAIN CL AND RESID 385:504)
209	X-RAY DIFFRACTION	209	(CHAIN CM AND RESID 1:189)
210	X-RAY DIFFRACTION	210	(CHAIN CM AND RESID 190:343)
211	X-RAY DIFFRACTION	211	(CHAIN CM AND RESID 344:384)
212	X-RAY DIFFRACTION	212	(CHAIN CM AND RESID 385:504)
213	X-RAY DIFFRACTION	213	(CHAIN CN AND RESID 1:189)
214	X-RAY DIFFRACTION	214	(CHAIN CN AND RESID 190:343)
215	X-RAY DIFFRACTION	215	(CHAIN CN AND RESID 344:384)
216	X-RAY DIFFRACTION	216	(CHAIN CN AND RESID 385:504)
217	X-RAY DIFFRACTION	217	(CHAIN CO AND RESID 1:189)
218	X-RAY DIFFRACTION	218	(CHAIN CO AND RESID 190:343)
219	X-RAY DIFFRACTION	219	(CHAIN CO AND RESID 344:384)
220	X-RAY DIFFRACTION	220	(CHAIN CO AND RESID 385:504)
221	X-RAY DIFFRACTION	221	(CHAIN CP AND RESID 1:189)
222	X-RAY DIFFRACTION	222	(CHAIN CP AND RESID 190:343)
223	X-RAY DIFFRACTION	223	(CHAIN CP AND RESID 344:384)
224	X-RAY DIFFRACTION	224	(CHAIN CP AND RESID 385:504)
225	X-RAY DIFFRACTION	225	(CHAIN CQ AND RESID 1:189)
226	X-RAY DIFFRACTION	226	(CHAIN CQ AND RESID 190:343)
227	X-RAY DIFFRACTION	227	(CHAIN CQ AND RESID 344:384)
228	X-RAY DIFFRACTION	228	(CHAIN CQ AND RESID 385:504)
229	X-RAY DIFFRACTION	229	(CHAIN CR AND RESID 1:189)
230	X-RAY DIFFRACTION	230	(CHAIN CR AND RESID 190:343)
231	X-RAY DIFFRACTION	231	(CHAIN CR AND RESID 344:384)
232	X-RAY DIFFRACTION	232	(CHAIN CR AND RESID 385:504)
233	X-RAY DIFFRACTION	233	(CHAIN CS AND RESID 1:189)
234	X-RAY DIFFRACTION	234	(CHAIN CS AND RESID 190:343)
235	X-RAY DIFFRACTION	235	(CHAIN CS AND RESID 344:384)
236	X-RAY DIFFRACTION	236	(CHAIN CS AND RESID 385:504)
237	X-RAY DIFFRACTION	237	(CHAIN CT AND RESID 1:189)
238	X-RAY DIFFRACTION	238	(CHAIN CT AND RESID 190:343)
239	X-RAY DIFFRACTION	239	(CHAIN CT AND RESID 344:384)
240	X-RAY DIFFRACTION	240	(CHAIN CT AND RESID 385:504)