ソフトウェア 名称 バージョン 分類 HKL-3000データ収集 MOLREP位相決定 REFMAC5.5.0066精密化 HKL-3000データ削減 HKL-3000データスケーリング
精密化 構造決定の手法 : 分子置換開始モデル : pdb entry 3KWM解像度 : 1.65→36.63 Å / Cor.coef. Fo :Fc : 0.971 / Cor.coef. Fo :Fc free : 0.959 / SU B : 3.355 / SU ML : 0.053 / 交差検証法 : THROUGHOUT / ESU R : 0.083 / ESU R Free : 0.085 / 立体化学のターゲット値 : MAXIMUM LIKELIHOOD / 詳細 : HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONSRfactor 反射数 %反射 Selection details Rfree 0.18207 2602 5.1 % RANDOM Rwork 0.14781 - - - obs 0.14962 48581 98.86 % -
溶媒の処理 イオンプローブ半径 : 0.8 Å / 減衰半径 : 0.8 Å / VDWプローブ半径 : 1.4 Å / 溶媒モデル : MASK原子変位パラメータ Biso mean : 27.123 Å2 Baniso -1 Baniso -2 Baniso -3 1- -0.31 Å2 0 Å2 -0.25 Å2 2- - -0.03 Å2 0 Å2 3- - - 0.29 Å2
精密化ステップ サイクル : LAST / 解像度 : 1.65→36.63 Åタンパク質 核酸 リガンド 溶媒 全体 原子数 3299 0 36 263 3598
拘束条件 大きな表を表示 (5 x 33) 大きな表を隠す Refine-ID タイプ Dev ideal Dev ideal target 数 X-RAY DIFFRACTION r_bond_refined_d0.015 0.022 3484 X-RAY DIFFRACTION r_bond_other_d0 0.02 3284 X-RAY DIFFRACTION r_angle_refined_deg1.409 1.991 4736 X-RAY DIFFRACTION r_angle_other_deg0.662 3 7690 X-RAY DIFFRACTION r_dihedral_angle_1_deg6.072 5 458 X-RAY DIFFRACTION r_dihedral_angle_2_deg42.513 26.277 137 X-RAY DIFFRACTION r_dihedral_angle_3_deg11.647 15 649 X-RAY DIFFRACTION r_dihedral_angle_4_deg5.143 15 13 X-RAY DIFFRACTION r_chiral_restr0.085 0.2 578 X-RAY DIFFRACTION r_gen_planes_refined0.007 0.02 3871 X-RAY DIFFRACTION r_gen_planes_other0.001 0.02 602 X-RAY DIFFRACTION r_nbd_refinedX-RAY DIFFRACTION r_nbd_otherX-RAY DIFFRACTION r_nbtor_refinedX-RAY DIFFRACTION r_nbtor_otherX-RAY DIFFRACTION r_xyhbond_nbd_refinedX-RAY DIFFRACTION r_xyhbond_nbd_otherX-RAY DIFFRACTION r_metal_ion_refinedX-RAY DIFFRACTION r_metal_ion_otherX-RAY DIFFRACTION r_symmetry_vdw_refinedX-RAY DIFFRACTION r_symmetry_vdw_otherX-RAY DIFFRACTION r_symmetry_hbond_refinedX-RAY DIFFRACTION r_symmetry_hbond_otherX-RAY DIFFRACTION r_symmetry_metal_ion_refinedX-RAY DIFFRACTION r_symmetry_metal_ion_otherX-RAY DIFFRACTION r_mcbond_it2.528 1.5 2228 X-RAY DIFFRACTION r_mcbond_other0.992 1.5 918 X-RAY DIFFRACTION r_mcangle_it3.882 2 3640 X-RAY DIFFRACTION r_scbond_it5.96 3 1256 X-RAY DIFFRACTION r_scangle_it9.149 4.5 1096 X-RAY DIFFRACTION r_rigid_bond_restrX-RAY DIFFRACTION r_sphericity_freeX-RAY DIFFRACTION r_sphericity_bonded
LS精密化 シェル 解像度 : 1.65→1.693 Å / Total num. of bins used : 20 Rfactor 反射数 %反射 Rfree 0.287 166 - Rwork 0.231 3396 - obs - - 94.94 %
精密化 TLS 手法 : refined / Refine-ID : X-RAY DIFFRACTION
大きな表を表示 (25 x 40) 大きな表を隠す ID L11 (°2 )L12 (°2 )L13 (°2 )L22 (°2 )L23 (°2 )L33 (°2 )S11 (Å °)S12 (Å °)S13 (Å °)S21 (Å °)S22 (Å °)S23 (Å °)S31 (Å °)S32 (Å °)S33 (Å °)T11 (Å2 )T12 (Å2 )T13 (Å2 )T22 (Å2 )T23 (Å2 )T33 (Å2 )Origin x (Å)Origin y (Å)Origin z (Å)1 10.5516 -5.4483 -1.3363 3.5924 3.6611 14.627 0.0118 0.4358 0.5318 -0.1414 -0.1978 0.0257 -0.7446 -0.7196 0.186 0.1403 0.0774 -0.0098 0.2001 0.2351 0.4045 -2.492 11.905 12.21 2 1.891 -0.2299 0.5223 8.6199 0.8566 1.2524 -0.115 0.4122 0.0764 -0.4559 0.2491 0.1803 -0.0402 -0.0573 -0.1341 0.1112 -0.0202 -0.0025 0.1978 0.0507 0.0478 1.618 -1.244 10.196 3 1.4407 -1.9123 0.3607 3.3246 -0.0372 0.8105 0.051 0.0993 -0.0083 -0.0335 0.0026 0.0802 0.1537 -0.1387 -0.0536 0.084 -0.0429 0.0014 0.1731 0.0335 0.0662 1.537 -8.991 19.366 4 2.1771 0.7546 0.7951 3.3939 2.045 1.3022 -0.0515 0.3372 0.1844 0.0134 -0.0638 0.1512 0.011 -0.0076 0.1153 0.0671 -0.0032 -0.0069 0.1551 0.0219 0.0183 -4.499 -4.681 15.248 5 0.9044 -1.0881 0.6552 1.7934 1.3079 9.8813 0.1391 0.0189 -0.1279 -0.1464 -0.0891 0.1484 0.2837 -0.3979 -0.0499 0.0652 -0.0415 -0.0065 0.0575 -0.0239 0.0335 -1.604 -15.491 18.39 6 3.0634 -0.4711 0.1719 0.7756 -0.5412 2.0835 -0.0667 0.045 -0.061 0.0655 0.0519 0.038 0.0082 -0.1781 0.0148 0.0209 0.0042 0.0179 0.0863 -0.0059 0.0172 -6.821 -5.544 25.738 7 3.1158 -2.9033 2.695 2.9062 -3.0118 6.9565 0.2455 -0.2794 -0.1956 -0.1684 0.2201 0.1447 0.5241 -0.4936 -0.4656 0.1196 -0.0933 -0.0552 0.0938 0.0414 0.1022 -0.258 -15.89 29.433 8 0.758 0.8322 0.271 3.7846 0.6837 1.4926 0.0238 0.1415 -0.0561 0.0455 -0.0541 -0.0813 0.122 -0.1825 0.0303 0.052 0.0015 0.0244 0.0868 -0.0186 0.0286 6.769 -8.213 21.449 9 10.7014 -7.844 -2.8917 6.5923 0.2208 5.4939 0.1402 0.2871 0.5291 -0.0578 -0.1744 -0.4784 -0.324 0.0175 0.0342 0.1115 -0.0474 0.0389 0.0974 0.0189 0.06 17.827 6.563 18.764 10 0.8225 0.4403 0.0767 1.1182 -0.0717 1.2389 0.0441 0.0404 -0.0173 0.0281 -0.0138 -0.0313 -0.0403 -0.1041 -0.0303 0.0325 0.0146 0.0192 0.0485 0.0028 0.0156 9.969 -1.772 27.592 11 0.7501 -0.5841 0.0414 10.2913 -0.6156 1.8462 0.0069 0.1828 -0.0572 -0.1636 -0.1503 -0.0625 0.043 -0.0806 0.1434 0.0351 0.0095 0.0276 0.0733 -0.0223 0.0374 10.732 -7.699 17.546 12 6.0299 1.8154 2.4985 1.9015 1.2858 1.6068 -0.1848 0.2801 0.3051 -0.2039 0.1282 0.0231 -0.2423 0.0469 0.0566 0.0959 0.017 0.0221 0.045 0.0263 0.0279 11.805 9.057 17.396 13 0.221 -0.2211 -0.2467 1.6177 -0.8099 1.2414 -0.0274 -0.0165 0.0029 0.157 -0.0115 -0.0394 -0.1704 -0.0578 0.0389 0.0927 0.0413 0.003 0.0631 -0.0149 0.0212 12.183 7.344 41.28 14 10.3107 3.3843 2.3052 4.9657 -1.1093 2.1972 -0.1247 0.1383 0.3308 0.4129 -0.0967 -0.0086 -0.4987 0.0675 0.2214 0.1619 -0.0071 -0.0346 0.0313 -0.0066 0.037 12.989 12.844 40.19 15 2.5316 2.5585 0.0058 3.5488 -0.7487 1.0162 0.0034 -0.1021 0.0829 0.1284 -0.0366 0.046 -0.1823 -0.1998 0.0332 0.0791 0.0384 0.0267 0.0654 -0.0118 0.0309 6.652 7.369 37.827 16 5.0933 -2.8865 -1.2693 9.409 6.085 4.0242 0.1443 0.1617 0.3942 -0.5541 0.1089 -0.4694 -0.3614 0.0987 -0.2532 0.0614 -0.001 0.0437 0.0434 0.0178 0.0647 23.793 7.083 28.926 17 2.2804 -2.1717 1.3624 3.3728 -1.8702 3.2979 -0.0689 -0.0346 0.1125 0.1066 0.0092 -0.1313 -0.0899 0.0519 0.0598 0.031 0.0049 0.0158 0.0207 -0.002 0.0214 21.434 1.228 36.344 18 0.6964 0.0791 0.0282 0.4507 0.7793 1.4342 0.0234 0.0359 -0.0641 -0.0069 0.029 -0.0658 0.0139 0.0108 -0.0525 0.049 0.0244 0.0334 0.0591 -0.0121 0.0545 15.694 -0.817 29.602 19 5.4587 -4.1591 1.2006 13.0069 -3.5449 3.1703 -0.0121 0.2903 0.2218 -0.406 0.1859 0.4537 -0.1105 0.1112 -0.1738 0.0673 -0.008 -0.0133 0.0813 0.0424 0.0523 7.149 8.167 8.417 20 1.4816 -1.0441 2.5274 12.8162 -3.3442 4.5185 -0.1545 0.3177 0.2371 -0.4262 -0.2711 -0.3861 -0.2064 0.5246 0.4256 0.1158 0.0317 0.0142 0.1822 0.0738 0.0529 10.021 4.175 7.107 21 0.5009 1.1732 0.6066 2.7903 1.6347 1.821 0.1791 0.0525 0.1986 0.4882 0.1239 0.3646 0.5042 0.0273 -0.303 0.2647 0.0179 -0.0186 0.2765 0.1433 0.4043 21.944 -12.34 73.963 22 2.0504 -4.7332 0.9778 12.7319 -0.9834 1.4501 -0.3631 -0.3105 0.2093 0.483 0.457 -0.6721 -0.3861 -0.2196 -0.0939 0.1593 0.0978 -0.0293 0.2182 -0.0559 0.0804 24.144 0.085 71.497 23 2.8647 -1.1449 0.9886 10.2617 3.7924 2.8331 0.1201 -0.5486 0.2469 0.4595 -0.371 0.2624 0.001 -0.526 0.251 0.1901 0.0019 0.028 0.2021 -0.0713 0.0556 17.399 5.574 65.247 24 10.5596 -2.8037 -5.7214 2.5456 2.7671 5.0413 -0.4833 -1.0282 -1.4327 0.1654 0.0951 0.001 0.2713 -0.0584 0.3882 0.1254 0.0643 0.0631 0.4303 0.2077 0.2968 14.831 -6.14 69.674 25 9.3692 -2.4 -0.5111 7.8186 -2.5667 4.7654 0.0618 -1.0989 0.4858 0.4361 0.4171 0.1762 -0.4932 0.4651 -0.4789 0.2025 0.0449 0.0222 0.3472 -0.1428 0.0843 15.853 5.824 73.696 26 10.0198 -0.4155 -2.7995 1.6713 -0.7389 3.6672 -0.2662 0.1821 -0.5256 0.2125 -0.0472 0.2121 -0.1226 -0.8204 0.3134 0.1224 0.0288 0.0674 0.3107 -0.0791 0.1069 7.651 -1.07 65.031 27 0.8641 0.5149 -0.9122 0.3701 0.3499 13.6597 0.1471 0.0806 0.1027 0.0838 0.0493 0.0538 -0.2186 -0.2069 -0.1964 0.0642 0.0655 0.0191 0.1315 -0.0066 0.0194 7.113 4.706 63.929 28 10.8839 -0.4351 6.3956 1.9136 -0.2061 4.0669 -0.5121 0.0626 0.4637 0.1779 0.138 -0.0689 -0.2577 0.0387 0.3741 0.1192 0.0298 0.0075 0.057 -0.0213 0.0767 11.25 8.813 55.124 29 1.0072 -0.6769 -0.5341 2.0011 1.3511 1.8395 -0.0308 -0.1055 0.0606 0.1946 -0.0362 -0.0522 0.0517 -0.0316 0.0669 0.0413 -0.0061 -0.0068 0.0564 -0.0039 0.0182 22.594 -5.767 58.899 30 0.3233 -0.5171 0.3282 1.1501 -0.1749 0.8067 -0.021 -0.0391 -0.0048 0.0738 0.008 0.0355 -0.044 -0.0641 0.013 0.0473 -0.01 0.0171 0.0777 0.0011 0.0079 18.986 -6.317 52.906 31 2.6205 -2.1412 3.1565 9.1244 -4.2402 4.9103 0.1051 -0.2107 0.0034 0.2493 0.0384 -0.1748 0.1128 -0.0726 -0.1434 0.0641 0.002 -0.0042 0.1036 -0.0263 0.0601 25.003 -5.29 61.812 32 2.8661 -1.0588 0.905 6.0427 1.1194 1.8605 0.1657 -0.0567 -0.4738 0.4519 -0.0437 -0.7237 0.3483 -0.0288 -0.122 0.1374 -0.0031 -0.0771 0.0913 0.0344 0.2774 28.454 -18.026 55.038 33 0.7911 -0.4623 0.6645 0.7958 0.0279 1.6699 0.0861 -0.0313 -0.0385 -0.0433 -0.0057 0.0421 0.0733 -0.0897 -0.0804 0.0381 -0.0109 0.0144 0.0166 0.007 0.0246 12.545 -14.699 39.407 34 3.9399 -1.4443 -1.9029 2.9378 -0.2604 4.1484 0.0914 -0.0308 0.0613 -0.0898 0.0935 -0.068 0.4079 0.0246 -0.185 0.0866 -0.0151 -0.0118 0.0245 -0.0114 0.0393 16.32 -20.143 39.959 35 5.5794 2.6139 -0.6558 4.7461 -2.0622 0.9572 0.1835 -0.3206 -0.0569 0.0784 -0.1563 0.1002 -0.0018 0.0323 -0.0272 0.0879 -0.0171 0.0775 0.1321 0.01 0.0829 3.785 -13.6 48.514 36 5.2815 -4.5734 0.9215 4.4874 0.3557 2.7105 0.2726 -0.1542 -0.1275 -0.2104 0.0004 0.0089 0.0985 -0.278 -0.273 0.0585 -0.0249 0.0195 0.0686 0.0091 0.0533 10.786 -15.124 44.324 37 10.8705 5.8387 0.0497 4.3381 -1.1852 2.4063 -0.1194 0.4096 -0.117 -0.0225 0.1397 -0.0363 0.2136 0.2769 -0.0203 0.0924 0.0228 0.0021 0.0618 -0.009 0.0217 25.024 -20.739 44.81 38 7.8781 -0.3832 4.8878 10.0289 -5.785 6.1072 0.2326 0.3404 -0.0676 -0.2047 -0.4867 -0.5295 0.2465 0.4764 0.2541 0.035 0.0204 0.0302 0.0899 0.029 0.0513 30.046 -10.723 43.163 39 1.5603 0.6506 0.4829 0.4954 -0.3404 1.8015 0.0636 0.0206 0.047 -0.0175 -0.0407 0.0221 0.0878 0.0932 -0.0229 0.0367 0.009 0.0201 0.0442 -0.0029 0.0153 20.394 -7.827 41.739 40 0.6626 -2.08 1.7355 7.129 -6.3622 10.288 -0.055 -0.0628 0.1245 0.1494 0.1221 -0.3908 0.2525 0.182 -0.0671 0.0388 0.0145 -0.0452 0.0928 -0.0223 0.0607 29.949 -9.703 64.97
精密化 TLSグループ 大きな表を表示 (5 x 40) 大きな表を隠す ID Refine-ID Refine TLS-ID Auth asym-ID Auth seq-ID 1 X-RAY DIFFRACTION 1 A7 - 11 2 X-RAY DIFFRACTION 2 A12 - 25 3 X-RAY DIFFRACTION 3 A26 - 36 4 X-RAY DIFFRACTION 4 A37 - 49 5 X-RAY DIFFRACTION 5 A50 - 56 6 X-RAY DIFFRACTION 6 A57 - 71 7 X-RAY DIFFRACTION 7 A72 - 78 8 X-RAY DIFFRACTION 8 A79 - 90 9 X-RAY DIFFRACTION 9 A91 - 95 10 X-RAY DIFFRACTION 10 A96 - 116 11 X-RAY DIFFRACTION 11 A117 - 121 12 X-RAY DIFFRACTION 12 A122 - 132 13 X-RAY DIFFRACTION 13 A133 - 152 14 X-RAY DIFFRACTION 14 A153 - 164 15 X-RAY DIFFRACTION 15 A165 - 180 16 X-RAY DIFFRACTION 16 A181 - 188 17 X-RAY DIFFRACTION 17 A189 - 194 18 X-RAY DIFFRACTION 18 A195 - 212 19 X-RAY DIFFRACTION 19 A213 - 218 20 X-RAY DIFFRACTION 20 A219 - 224 21 X-RAY DIFFRACTION 21 B10 - 17 22 X-RAY DIFFRACTION 22 B18 - 25 23 X-RAY DIFFRACTION 23 B26 - 33 24 X-RAY DIFFRACTION 24 B34 - 46 25 X-RAY DIFFRACTION 25 B47 - 52 26 X-RAY DIFFRACTION 26 B53 - 70 27 X-RAY DIFFRACTION 27 B71 - 75 28 X-RAY DIFFRACTION 28 B76 - 81 29 X-RAY DIFFRACTION 29 B82 - 94 30 X-RAY DIFFRACTION 30 B95 - 116 31 X-RAY DIFFRACTION 31 B117 - 125 32 X-RAY DIFFRACTION 32 B126 - 134 33 X-RAY DIFFRACTION 33 B135 - 152 34 X-RAY DIFFRACTION 34 B153 - 163 35 X-RAY DIFFRACTION 35 B164 - 170 36 X-RAY DIFFRACTION 36 B171 - 177 37 X-RAY DIFFRACTION 37 B178 - 182 38 X-RAY DIFFRACTION 38 B183 - 188 39 X-RAY DIFFRACTION 39 B189 - 206 40 X-RAY DIFFRACTION 40 B207 - 224