温度: 298 K / 手法: sitting drop vapor diffuction / pH: 7 詳細: Protein (10 mM Hepes pH 7.5, 150 mM NaCl, 10% glycerol, 1 mM DTT, 5 mM MgCl); Reservoir (0.1 M Bis-Tris Propane:HCl, 1.8 M Magnesium Sulfate); Cryoprotection (Reservoir, + 20% glycerol), ...詳細: Protein (10 mM Hepes pH 7.5, 150 mM NaCl, 10% glycerol, 1 mM DTT, 5 mM MgCl); Reservoir (0.1 M Bis-Tris Propane:HCl, 1.8 M Magnesium Sulfate); Cryoprotection (Reservoir, + 20% glycerol), sitting drop vapor diffuction, temperature 298K
解像度: 1.7→26.588 Å / Occupancy max: 1 / Occupancy min: 0.06 / FOM work R set: 0.8836 / SU ML: 0.17 / σ(F): 0 / σ(I): 0 / 位相誤差: 18.81 / 立体化学のターゲット値: ML 詳細: THE STRUCTURE WAS REFINED UTILIZING THE STRUCTURE AND GEOMETRIC RESTRAINTS OF BENOZIC ACID, HOWEVER THE EXPERIMENTERS CAN NOT BE CERTAIN OF THE LIGANDS IDENTITY AS BENZOIC ACID WAS NOT A ...詳細: THE STRUCTURE WAS REFINED UTILIZING THE STRUCTURE AND GEOMETRIC RESTRAINTS OF BENOZIC ACID, HOWEVER THE EXPERIMENTERS CAN NOT BE CERTAIN OF THE LIGANDS IDENTITY AS BENZOIC ACID WAS NOT A COMPONENT OF THE CRYSTALLIZATION OR PURIFICATION.
Rfactor
反射数
%反射
Selection details
Rfree
0.2038
1527
5.06 %
RANDOM
Rwork
0.1655
-
-
-
all
0.1673
30180
-
-
obs
0.1673
30180
99.85 %
-
溶媒の処理
減衰半径: 0.8 Å / VDWプローブ半径: 1.1 Å / 溶媒モデル: FLAT BULK SOLVENT MODEL