COBALT (II) ION (CO): COBALT MOST LIKELY GIVEN THE ANOMALOUS SIGNAL AT TWO DIFFERENT WAVELENGTHS ...COBALT (II) ION (CO): COBALT MOST LIKELY GIVEN THE ANOMALOUS SIGNAL AT TWO DIFFERENT WAVELENGTHS GLYCEROL (GOL): TENTATIVE. SOME DENSITY IN THE ACTIVE SITE RUTHENIUM COMPOUND NOT OBSERVED IN ELECTRON DENSITY: BIS (2,2'-BIPYRIDINE)-4,4'-DICARBOXY-BIPYRIDINE-RUTHENIUM DI(N-SUCCINIMIDYL ESTER) BIS (HEXAFLUOROPHOSPHATE)
-
実験情報
-
実験
実験
手法: X線回折 / 使用した結晶の数: 10
-
試料調製
結晶
マシュー密度: 2.7 Å3/Da / 溶媒含有率: 54 % 解説: STRUCTURE FACTOR FILE CONTAINS DATA TILL 0.897 ANGSTROM.
結晶化
pH: 7 詳細: 28.7 MG/ML PROTEIN, 1.4 MG/ML PROTEIN COVALENTLY LABELED WITH A RUTHENIUM-CONTAINING LABEL, 0.9 M AMMONIUM SULPHATE, 100 MM HEPES PH 7.0
解像度: 1.42→70.77 Å / Cor.coef. Fo:Fc: 0.977 / Cor.coef. Fo:Fc free: 0.968 / SU B: 1.021 / SU ML: 0.019 / 交差検証法: THROUGHOUT / ESU R: 0.04 / ESU R Free: 0.039 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. U VALUES REFINED INDIVIDUALLY
Rfactor
反射数
%反射
Selection details
Rfree
0.12971
4334
5 %
RANDOM
Rwork
0.10291
-
-
-
obs
0.10426
82705
99.93 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: BABINET MODEL WITH MASK