7P0W
Crystal structure of a trapped Pab-AGOG/double-standed DNA covalent intermediate (DNA containing thymine opposite to lesion)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-05-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97856 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 59.776, 71.578, 138.691 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.650 - 1.120 |
R-factor | 0.1249 |
Rwork | 0.124 |
R-free | 0.14300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7oy7 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHASER (2.8.3) |
Refinement software | PHENIX (1.19_4092) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.880 | 1.140 |
High resolution limit [Å] | 1.120 | 1.120 |
Rmerge | 0.064 | 0.598 |
Number of reflections | 114280 | 5266 |
<I/σ(I)> | 17.7 | 2.3 |
Completeness [%] | 99.4 | |
Redundancy | 12.6 | |
CC(1/2) | 0.999 | 0.834 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | MgCl2, Na acetate pH5.0, MPD |