6PAW
Crystal structure of DAPK2 S308A Calcium/Calmodulin complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-06-06 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 89.440, 95.880, 263.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 131.650 - 2.953 |
R-factor | 0.2506 |
Rwork | 0.249 |
R-free | 0.28840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB entries 2A2A & 1ZUZ |
Data reduction software | XDS (November 3, 2014) |
Data scaling software | XSCALE (November 3, 2014 BUILT=20141118) |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 131.650 | 3.200 |
High resolution limit [Å] | 2.950 | 2.950 |
Rmerge | 0.275 | 1.853 |
Number of reflections | 48427 | 1250 |
<I/σ(I)> | 9.5 | 1.4 |
Completeness [%] | 64.4 | |
Redundancy | 8.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 292.15 | 0.1 M Bis-Tris-HCl, pH 6.5, 0.6 M sodium chloride, 14.3% PEG3350 |