6GEK
TEAD4 (216-434);Y429F COMPLEXED WITH YAP PEPTIDE (60-100) AND MYRISTOATE (COVALENTLY BOUND) AT 2.28A (P212121 CRYSTAL FORM); MYRISTOYLATION WAS DONE BY ADDING MYR-COA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-09 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.99999 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.236, 77.041, 164.033 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.900 - 2.280 |
R-factor | 0.2209 |
Rwork | 0.220 |
R-free | 0.24650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ge3 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.951 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.900 | 2.340 |
High resolution limit [Å] | 2.280 | 2.280 |
Rmerge | 0.111 | 0.651 |
Rmeas | 0.121 | 0.704 |
Total number of observations | 163458 | |
Number of reflections | 25747 | |
<I/σ(I)> | 12.1 | 2.7 |
Completeness [%] | 99.7 | 100 |
Redundancy | 6.3 | 6.9 |
CC(1/2) | 0.997 | 0.885 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | 25% PEG 3350, 0.2M MgCl2, 0.1M Bis-TRIS |