6GEE
TEAD4 (216-434);E263A COMPLEXED WITH YAP PEPTIDE (60-100); S94A AND MYRISTOATE (COVALENTLY BOUND) AT 1.96A (P41212 CRYSTAL FORM); MYRISTOYLATION WAS DONE BY ADDING MYR-COA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-02-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.99994 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 59.315, 59.315, 158.310 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.790 - 1.960 |
R-factor | 0.2176 |
Rwork | 0.216 |
R-free | 0.24500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ge3 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.950 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.790 | 2.010 |
High resolution limit [Å] | 1.960 | 1.960 |
Rmerge | 0.116 | 0.982 |
Number of reflections | 21126 | |
<I/σ(I)> | 16.4 | 3 |
Completeness [%] | 99.8 | 100 |
Redundancy | 12.7 | 13.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | 17% PEG 10000, 0.1M ammonium acetate, 0.1M Bis-TRIS |