6CPR
Crystal structure of 4-1BBL/4-1BB complex in C2 space group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-01-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 115.280, 66.504, 129.356 |
Unit cell angles | 90.00, 103.09, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 38.000 | 38.000 | 2.770 |
High resolution limit [Å] | 2.700 | 12.080 | 2.700 |
Rmerge | 0.143 | 0.078 | 0.921 |
Rmeas | 0.156 | 0.085 | 1.022 |
Total number of observations | 148726 | ||
Number of reflections | 25892 | 308 | 1894 |
<I/σ(I)> | 7.8 | 17.63 | 1.95 |
Completeness [%] | 97.7 | 93.6 | 95.4 |
Redundancy | 5.744 | 5.328 | 5.016 |
CC(1/2) | 0.993 | 0.994 | 0.817 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.1 M Na acetate pH 4.6 10% W/V PEG 4000 0.2M Ammonium sulfate |