6CDF

Human CtBP1 (28-378)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	CCD
Collection date	2016-09-01
Detector	RIGAKU SATURN 944
Wavelength(s)	1.54178
Spacegroup name	P 64 2 2
Unit cell lengths	88.657, 88.657, 163.914
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	38.991 - 2.600
R-factor	0.2088
Rwork	0.207
R-free	0.24450
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4u6q
RMSD bond length	0.003
RMSD bond angle	0.665
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.10_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.690
High resolution limit [Å]	2.600	2.600
Number of reflections	15115
<I/σ(I)>	30.5
Completeness [%]	95.8
Redundancy	7.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	293	5% PEG400, 140 mM calcium chloride