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5Z0M

Crystal structure of copper-bound H63F-mutated tyrosinase from Streptomyces castaneoglobisporus in complex with the caddie protein obtained by soaking in the hydroxylamine-containing solution for 12 h at 298 K

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL26B2
Synchrotron siteSPring-8
BeamlineBL26B2
Temperature [K]100
Detector technologyCCD
Collection date2011-01-25
DetectorRAYONIX MX-225
Wavelength(s)0.9000
Spacegroup nameP 21 21 2
Unit cell lengths64.910, 97.350, 54.920
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.000 - 1.700
R-factor0.1422
R-free0.20660
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle0.025
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareCNS
Refinement softwareSHELXL-97
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]100.0001.760
High resolution limit [Å]1.7001.700
Rmerge0.0580.442
Number of reflections355443515
<I/σ(I)>28.82.7
Completeness [%]90.791.8
Redundancy65.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.5298PEG 3350, SODIUM NITRATE, HEPES

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