5YXY
Crystal structure of the HyhL-HypA complex (form I)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Temperature [K] | 95 |
Detector technology | PIXEL |
Collection date | 2014-06-06 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.1 |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 245.309, 261.427, 134.870 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.220 - 3.299 |
R-factor | 0.3058 |
Rwork | 0.305 |
R-free | 0.32120 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.925 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.220 | 3.500 |
High resolution limit [Å] | 3.299 | 3.300 |
Rmerge | 0.151 | 0.800 |
Number of reflections | 64828 | |
<I/σ(I)> | 12.3 | |
Completeness [%] | 99.0 | |
Redundancy | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1M NaCl, 0.1M MgCl2, 10% PEG 3350, 0.1M imidazole-HCl (pH 6.2) |