Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-01-01 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.00002 |
Spacegroup name | P 41 21 2 |
格子定数 [Å] | 57.850, 57.850, 366.480 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 57.000 - 3.400 |
R因子 | 0.2584 |
Rwork | 0.255 |
R-free | 0.29590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4OE8 |
結合長の平均二乗偏差(RMSD) [Å] | 0.004 |
結合角の平均二乗偏差(RMSD) [度] | 0.850 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 57.000 | 3.500 |
分解能 [Å] (高) | 3.400 | 3.400 |
Rmeas | 0.116 | 0.921 |
独立反射数 | 9551 | |
<I/σ(I)> | 20.7 | 5.2 |
完全性 [%] | 99.8 | 100 |
冗長性 | 22.29 | 23.4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 7.3 | 294 | 0.2M POTASSIUM FORMATE, 20.75% W/V PEG 3350, PH 7.3 |