Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-01-01 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.00002 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.960, 56.740, 100.070 |
Unit cell angles | 90.00, 99.73, 90.00 |
Refinement procedure
Resolution | 40.610 - 1.740 |
Rwork | 0.165 |
R-free | 0.19800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3duh |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.3_1479) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.000 | 1.850 |
High resolution limit [Å] | 1.740 | 1.740 |
Rmeas | 0.054 | 0.636 |
Number of reflections | 63104 | |
<I/σ(I)> | 13.7 | 1.8 |
Completeness [%] | 97.9 | 91.1 |
Redundancy | 3.4 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 294 | 20.75% PEG 3350, 200MM SODIUM SULPHATE |