Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-06-14 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97892 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 85.450, 103.310, 256.030 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 45.896 - 3.600 |
| R-factor | 0.2172 |
| Rwork | 0.215 |
| R-free | 0.26290 |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.605 |
| Refinement software | PHENIX (dev_2376) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.900 | |
| High resolution limit [Å] | 3.600 | 3.600 |
| Number of reflections | 26960 | |
| <I/σ(I)> | 13.2 | |
| Completeness [%] | 99.6 | |
| Redundancy | 4.61 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.4 | 293 | 0.9 M sodium citrate pH 6.4, 0.25 M potassium chloride, 1% v/v ethanol, 3 % v/v acetonitrile, 6 % v/v ethylene glycol and 10 mM spermidine |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.4 | 293 | 0.9 M sodium citrate pH 6.4, 0.25 M potassium chloride, 1% v/v ethanol, 3 % v/v acetonitrile, 6 % v/v ethylene glycol and 10 mM spermidine |
