5I32
Ammonia permeable aquaporin AtTIP2;1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-02-05 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1 |
Spacegroup name | I 4 |
Unit cell lengths | 89.270, 89.270, 82.491 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.630 - 1.180 |
R-factor | 0.10413 |
Rwork | 0.104 |
R-free | 0.11538 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3gd8 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.357 |
Data reduction software | XDS |
Data scaling software | SCALA (3.3.20) |
Phasing software | MOLREP (11.0.02) |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.630 | 1.220 |
High resolution limit [Å] | 1.180 | 1.180 |
Rmerge | 0.075 | 1.170 |
Number of reflections | 105884 | |
<I/σ(I)> | 12.65 | 1.63 |
Completeness [%] | 99.6 | 97.6 |
Redundancy | 13.2 | 10.8 |
CC(1/2) | 1.000 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 295 | 50 mM magnesium/sodium acetate pH 5.0 and 28% (v/v) PEG 400 |