5HO6
CRYSTAL STRUCTURE OF CMET IN COMPLEX WITH CMPD.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-01-15 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0723 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.550, 46.750, 157.751 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.940 - 1.970 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 34.940 |
High resolution limit [Å] | 1.970 |
Number of reflections | 21871 |
<I/σ(I)> | 13.9 |
Completeness [%] | 97.1 |
Redundancy | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 277 | Tris 100mM - MPD 20% - pH8.5 |