5HDG
crystal structure of heat shock factor 1-DBD
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-07-06 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97915 |
Spacegroup name | I 2 2 2 |
格子定数 [Å] | 48.610, 64.420, 68.770 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 32.210 - 1.700 |
R因子 | 0.1935 |
Rwork | 0.191 |
R-free | 0.21840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3hts |
結合長の平均二乗偏差(RMSD) [Å] | 0.003 |
結合角の平均二乗偏差(RMSD) [度] | 0.753 |
Data reduction software | XSCALE |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 32.210 | 1.730 |
分解能 [Å] (高) | 1.700 | 1.700 |
Rmerge_l_obs | 0.120 | 0.527 |
独立反射数 | 12343 | |
<I/σ(I)> | 4.1 | 3 |
完全性 [%] | 99.5 | 99.8 |
冗長性 | 7.1 | 7.3 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 293 | 0.2M sodium formate, pH 7.2, 22%(w/v) PEG3350 |