5B6B
Complex of LATS1 and phosphomimetic MOB1b
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-11-12 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.9 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 168.646, 301.437, 127.379 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.644 - 3.536 |
R-factor | 0.2245 |
Rwork | 0.222 |
R-free | 0.26560 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5b5w |
RMSD bond length | 0.005 |
RMSD bond angle | 1.042 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | HKL-2000 |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 30.000 |
High resolution limit [Å] | 3.500 | 3.560 |
Rmerge | 0.147 | |
Number of reflections | 41452 | |
<I/σ(I)> | 19.9 | |
Completeness [%] | 100.0 | |
Redundancy | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | PEG 3350, sodium sulfate |