4PLK
Hepatitis E Virus E2s domain (Genotype I) in complex with a neutralizing antibody 8G12
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-12-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.196, 191.993, 192.584 |
Unit cell angles | 90.00, 90.03, 90.00 |
Refinement procedure
Resolution | 33.992 - 4.000 |
R-factor | 0.2662 |
Rwork | 0.264 |
R-free | 0.29610 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.580 |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 33.992 |
High resolution limit [Å] | 4.000 |
Number of reflections | 31821 |
<I/σ(I)> | 5.8 |
Completeness [%] | 90.5 |
Redundancy | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 294 | 12% PEG 5000, 0.05M NaH2PO4 |