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4KHW

Ternary complex of RB69 mutant L415F with ribonucleotide at -2 position

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-ID
Synchrotron siteAPS
Beamline22-ID
Temperature [K]95
Detector technologyCCD
Collection date2010-06-18
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)1.00
Spacegroup nameP 21 21 21
Unit cell lengths80.355, 118.630, 126.310
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution44.642 - 2.371
R-factor0.1743
Rwork0.172
R-free0.22410
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle0.764
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHENIX (1.7_650)
Refinement softwarePHENIX ((PHENIX.REFINE: 1.7_650))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.440
High resolution limit [Å]2.3712.370
Rmerge0.0700.453
Number of reflections44309
Completeness [%]98.798.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP729850 MM TRIS-HCL, 19% PEG350, 180 MM CALCIUM CHLORIDE,, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K

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