4CZY
Complex of Neurospora crassa PAN2 (WD40-CS1) with PAN3 (pseudokinase and C-term)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-16 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.266, 139.976, 157.444 |
Unit cell angles | 90.00, 97.81, 90.00 |
Refinement procedure
Resolution | 48.740 - 3.400 |
R-factor | 0.2233 |
Rwork | 0.221 |
R-free | 0.26290 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 4BWX AND 4CZX |
RMSD bond length | 0.004 |
RMSD bond angle | 0.958 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.740 | 3.590 |
High resolution limit [Å] | 3.390 | 3.390 |
Number of reflections | 33318 | |
<I/σ(I)> | 9.9 | 1.4 |
Completeness [%] | 99.0 | 94.8 |
Redundancy | 3.7 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 7% PEG 4000, 13% GLYCEROL, 0.1M MES/IMIDAZOLE (PH 6.5), 30MM SODIUM NITRATE, 30MM DI-SODIUM HYDROGEN PHOSPHATE, 30MM AMMONIUM SULFATE |