3UIR
Crystal structure of the plasmin-textilinin-1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ DW |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-12-05 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 81.901, 48.019, 82.627 |
Unit cell angles | 90.00, 102.08, 90.00 |
Refinement procedure
Resolution | 39.550 - 2.777 |
R-factor | 0.2111 |
Rwork | 0.209 |
R-free | 0.25800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.905 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | EPMR |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.600 | 2.890 |
High resolution limit [Å] | 2.777 | 2.780 |
Rmerge | 0.117 | 0.284 |
Number of reflections | 15858 | |
<I/σ(I)> | 7.9 | 3.6 |
Completeness [%] | 99.8 | 99.3 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.17M ammonium sulfate, 25.5% PEG 4000, 15% glycerol, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |