3S8W
D2 domain of human IFNAR2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-10-29 |
Detector | MARMOSAIC 325 mm CCD |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 82.660, 82.660, 225.330 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.925 - 2.600 |
Rwork | 0.218 |
R-free | 0.27000 |
Structure solution method | SAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.220 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | autoSHARP |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.925 | 2.700 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 26344 | |
<I/σ(I)> | 16.3 | 2.4 |
Completeness [%] | 99.4 | 99.2 |
Redundancy | 5.6 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 293 | 31% (w/v) PEG 4000, 200 mM Li2SO4, 100 mM Tris pH 8.5, 5% (v/v) MPD, 10 mM Na acetate, 1.5% (w/v) PEG8000, VAPOR DIFFUSION, HANGING DROP, temperature 293K |